4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride

Base Information

• Chemical Name: 4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride
• CAS No.: 13912-65-7
• Deprecated CAS: 184908-80-3,1383712-39-7,1610790-00-5
• Molecular Formula: C16H12 O6
• Molecular Weight: 300.268
• Hs Code.: 2917399090
• European Community (EC) Number: 678-141-8
• DSSTox Substance ID: DTXSID60884727
• Nikkaji Number: J111.210D
• Mol file: 13912-65-7.mol

Synonyms:13912-65-7;4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride;5-(2,5-Dioxotetrahydrofuran-3-yl)-4,5-dihydronaphtho[1,2-c]furan-1,3(3aH,9bH)-dione;4-(2,5-Dioxotetrahydrofuran-3-yl)-tetralin-1,2-dicarboxylic Anhydride;Tetralin dianhydride;5-(2,5-dioxooxolan-3-yl)-3a,4,5,9b-tetrahydrobenzo[e][2]benzofuran-1,3-dione;Naphtho[1,2-c]furan-1,3-dione, 3a,4,5,9b-tetrahydro-5-(tetrahydro-2,5-dioxo-3-furanyl)-;Naphtho(1,2-c)furan-1,3-dione, 3a,4,5,9b-tetrahydro-5-(tetrahydro-2,5-dioxo-3-furanyl)-;SCHEMBL257601;DTXSID60884727;MFCD00030105;AKOS015855824;AS-73964;FT-0636979;D78432;3-(3-Furan-2-yl-[1,2,4]oxadiazol-5-yl)-propionicacid;3-{1,3-dioxo-1H,3H,3aH,4H,5H,9bH-naphtho[1,2-c]furan-5-yl}oxolane-2,5-dione;4-(2,5-Dioxotetrahydro-3-furyl)-1,2,3,4-tetrahydro-1,2-naphthalenedicarboxylic anhydride;5-(2,5-Dioxotetrahydro-3-furanyl)-3a,4,5,9b-tetrahydronaphtho[1,2-c]furan-1,3-dione #;4-(2,5-dioxotetra-hydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic anhydride;4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride, >/=97%

Chemical Property of 4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride

Chemical Property:

• Melting Point: 204 °C
• Boiling Point: 589.4°Cat760mmHg
• Flash Point: 265.2°C
• PSA: 86.74000
• Density: 1.494g/cm³
• LogP: 1.04680
• Storage Temp.: Inert atmosphere,Room Temperature
• Solubility.: soluble in Dimethylformamide
• XLogP3: 0.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 300.06338810
• Heavy Atom Count: 22
• Complexity: 567

Purity/Quality:

98% ^*data from raw suppliers

4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Plastics & Rubber -> Acid Anhydrides, Cyclic
• Canonical SMILES: C1C(C2=CC=CC=C2C3C1C(=O)OC3=O)C4CC(=O)OC4=O

Technology Process of 4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride

There total 8 articles about 4-(2,5-Dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic Anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(1,2-dicarboxy-ethyl)-1,2,3,4-tetrahydro-naphthalene-1,2-dicarboxylic acid (106145-04-4) → 4-(2,5-dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic anhydride (13912-65-7)

Guidance literature:

With acetic anhydride; optically inactive stereoisomer(ic) of mp: 203 degree;

Reference yield:

4-(1,2-bis-methoxycarbonyl-ethyl)-1,2,3,4-tetrahydro-naphthalene-1,2-dicarboxylic acid dimethyl ester → 4-(2,5-dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic anhydride (13912-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous KOH; methanol

2: acetic acid anhydride

With methanol; potassium hydroxide; acetic anhydride;

Reference yield:

maleic anhydride (108-31-6) + styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → 4-(2,5-dioxotetrahydrofuran-3-yl)-1,2,3,4-tetrahydronaphthalene-1,2-dicarboxylic anhydride (13912-65-7)

Guidance literature:

With 2,4,6-Trinitrophenol; benzene; optically inactive stereoisomer(ic) of mp: 203 degree;

upstream raw materials:

maleic anhydride

styrene

4-(1,2-dicarboxy-ethyl)-1,2,3,4-tetrahydro-naphthalene-1,2-dicarboxylic acid

2,4,6-Trinitrophenol

Downstream raw materials:

naphtho[2,3-b]furan-2(3H)-one

acrylic acid

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