2-(4-fluorophenyl)-2,3-dihydro-1H-perimidine

Base Information

• Chemical Name: 2-(4-fluorophenyl)-2,3-dihydro-1H-perimidine
• CAS No.: 1813-69-0
• Molecular Formula: C17H13FN2
• Molecular Weight: 264.302

Synonyms:

Chemical Property of 2-(4-fluorophenyl)-2,3-dihydro-1H-perimidine

Chemical Property:

• Vapor Pressure: 7.11E-10mmHg at 25°C
• Boiling Point: 493.3°Cat760mmHg
• Flash Point: 252.1°C
• Density: 1.24g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-fluorophenyl)-2,3-dihydro-1H-perimidine

There total 3 articles about 2-(4-fluorophenyl)-2,3-dihydro-1H-perimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-fluorobenzaldehyde (459-57-4) + naphthalene-1,8-diamine (479-27-6) → 2-(4-fluorophenyl)-2,3-dihydro-1H-1H-2,3-dihydro1H-2,3-dihydroperimidine (1813-69-0)

Guidance literature:

With tribromide-modified silica-coated magnetic nanoparticles (Fe₃O₄/SiO₂/(CH₂)3N+Me₃Br₃); In neat (no solvent); at 80 ℃; for 0.166667h; Green chemistry;

DOI:10.1016/j.catcom.2014.09.046

Reference yield: 65.0%

4-fluorobenzylic alcohol (459-56-3) + naphthalene-1,8-diamine (479-27-6) → 2-(4-fluorophenyl)-2,3-dihydro-1H-1H-2,3-dihydro1H-2,3-dihydroperimidine (1813-69-0)

Guidance literature:

With C₁₃H₁₆MnN₂O₃S⁽¹⁺⁾*Br^(1-); potassium hydroxide; In toluene; at 140 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.organomet.9b00131

Reference yield:

→ 2-(4-fluorophenyl)-2,3-dihydro-1H-1H-2,3-dihydro1H-2,3-dihydroperimidine (1813-69-0)

Guidance literature:

4-Fluor-benzaldehyd, 1,8-Diamino-naphthalin, sd. abs. A. (20 min);

upstream raw materials:

4-fluorobenzaldehyde

naphthalene-1,8-diamine

4-fluorobenzylic alcohol

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