N,N'-Bis(isopropoxycarbonyl)-4-methyl-1,3-phenylenediamine

Base Information

Chemical Name:N,N'-Bis(isopropoxycarbonyl)-4-methyl-1,3-phenylenediamine
CAS No.:42592-07-4
Molecular Formula:C15H22 N2 O4
Molecular Weight:294.351
Hs Code.:2924299090
European Community (EC) Number:667-329-5
NSC Number:48104
DSSTox Substance ID:DTXSID20962590
Nikkaji Number:J580.580E
Wikidata:Q82944303
Mol file:42592-07-4.mol

Synonyms:42592-07-4;NSC48104;Oprea1_766744;SCHEMBL11080337;DTXSID20962590;SRHAONPLNDTLMO-UHFFFAOYSA-N;N,N'-BIS(ISOPROPOXYCARBONYL)-4-METHYL-1,3-PHENYLENEDIAMINE;NSC-48104;AKOS001743658;propan-2-yl N-(2-methyl-5-{[(propan-2-yloxy)carbonyl]amino}phenyl)carbamate;Diisopropyl N,N'-(4-methyl-m-phenylene)dicarbamate;1,3-Phenilenedicarbaminic acid, 4-methyl-, diisopropyl ester;Dipropan-2-yl (4-methyl-1,3-phenylene)bis(hydrogen carbonimidate);Carbamic acid, (4-methyl-1,3-phenylene)-, bis(1-methylethyl) ester;Propan-2-yl N-[2-methyl-5-(propan-2-yloxycarbonylamino)phenyl]carbamat e

Suppliers and Price of N,N'-Bis(isopropoxycarbonyl)-4-methyl-1,3-phenylenediamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N,N'-BIS(ISOPROPOXYCARBONYL)-4-METHYL-1,3-PHENYLENEDIAMINE 95.00%
5MG
$ 504.31

Total 5 raw suppliers

Chemical Property of N,N'-Bis(isopropoxycarbonyl)-4-methyl-1,3-phenylenediamine

Chemical Property:

Vapor Pressure:0.000171mmHg at 25°C
Boiling Point:330°Cat760mmHg
Flash Point:153.4°C
PSA：76.66000
Density:1.17g/cm³
LogP:4.05480
XLogP3:2.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:294.15795719
Heavy Atom Count:21
Complexity:358

Purity/Quality:

99% ^*data from raw suppliers

N,N'-BIS(ISOPROPOXYCARBONYL)-4-METHYL-1,3-PHENYLENEDIAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)NC(=O)OC(C)C)NC(=O)OC(C)C

Technology Process of N,N'-Bis(isopropoxycarbonyl)-4-methyl-1,3-phenylenediamine

There total 3 articles about N,N'-Bis(isopropoxycarbonyl)-4-methyl-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 67-63-0,8013-70-5
isopropyl alcohol

: 584-84-9,6144-18-9,26006-20-2
2,4-Toluene diisocyanate

: 42592-07-4
diisopropyl (4-methyl-1,3-phenylene)dicarbamate

Guidance literature:: isopropyl alcohol; With dibutyltin dilaurate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

2,4-Toluene diisocyanate; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/anie.201800795

Reference yield:

: 6935-99-5
2,4-bis(methoxycarbonylamino)toluene

: 42592-07-4
diisopropyl (4-methyl-1,3-phenylene)dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: montmorillonite K₁₀ Clay / 1-methyl-pyrrolidin-2-one / 0.5 h / 190 °C / Microwave irradiation

2: 0 - 20 °C

With montmorillonite K₁₀ Clay; In 1-methyl-pyrrolidin-2-one;
DOI:10.1080/00397911.2020.1762093