2-(4-Bromoanilino)acetohydrazide

Base Information

Chemical Name:2-(4-Bromoanilino)acetohydrazide
CAS No.:2371-33-7
Molecular Formula:C₈H₁₀BrN₃O
Molecular Weight:244.091
Hs Code.:
NSC Number:190330
DSSTox Substance ID:DTXSID70307179
Wikidata:Q82054538
Mol file:2371-33-7.mol

Synonyms:2-(4-bromoanilino)acetohydrazide;2371-33-7;2-(4-bromophenylamino)acetohydrazide;NSC190330;2-[(4-bromophenyl)amino]acetohydrazide (non-preferred name);DTXSID70307179;STK279212;AKOS000295995;NSC-190330;BB 0241513;(4-Bromo-phenylamino)-acetic acid hydrazide

Suppliers and Price of 2-(4-Bromoanilino)acetohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 2-(4-Bromoanilino)acetohydrazide

Chemical Property:

Vapor Pressure:2.6E-09mmHg at 25°C
Boiling Point:478.3°Cat760mmHg
Flash Point:243.1°C
PSA：67.15000
Density:1.614g/cm³
LogP:2.01510
XLogP3:1.7
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:243.00072
Heavy Atom Count:13
Complexity:169

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1NCC(=O)NN)Br

Technology Process of 2-(4-Bromoanilino)acetohydrazide

There total 5 articles about 2-(4-Bromoanilino)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 213995-52-9
2-(4-bromophenylamino)acetamide

: 2371-33-7
2-(4-bromophenylamino)acetohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; Reflux;
DOI:10.1007/s00044-011-9924-6

Reference yield:

: 2521-92-8
ethyl 2-((4-bromophenyl)amino)acetate

: 2371-33-7
2-(4-bromophenylamino)acetohydrazide

Guidance literature:: With hydrazine;
DOI:10.1021/jo01096a009

Reference yield:

: 106-40-1
4-bromo-aniline

: 2371-33-7
2-(4-bromophenylamino)acetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / ethanol / 4 h / Heating

2: sulphuric acid / benzene / 14 h / Heating

3: hydrazinehydrate / H₂O; ethanol / 5 h / Heating

With sulfuric acid; sodium carbonate; hydrazine hydrate; In ethanol; water; benzene;