Technology Process of Einecs 234-648-2
There total 21 articles about Einecs 234-648-2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
water;
chlorides and C6H5Na3O7*2H2O, mixed, dissolved in water; soln. added dropwise to aq. alkaline NaBH4 soln. under strong stirring at room temp.; aged 6 h in water bath at 80°C; filtered, washed with water and acetone for 3 times; dried at 105°C for 24 h under vac.;
DOI:10.1016/j.jallcom.2008.11.159
- Guidance literature:
-
With
KBH4; H(OCH2CH2)nOH;
In
water;
byproducts: H2, CuH(x), SnH(x); High Pressure; mixing CuCl2 and SnCl2 (1.2:1), addn. of water, addn. of KBH4 and polyethylene glycol (average molecular weight 600 or 20000), heating to 80°C in autoclave; cooling to room temp. after 5 h, centrifugation, washing with water, washing with ethanol, drying at 100°C under vacuum for 24 h, XRD;
DOI:10.1016/j.poly.2010.02.035