4,4'-[(1e)-3-Methyltriaz-1-ene-1,3-diyl]dibenzonitrile

Base Information

Chemical Name:4,4'-[(1e)-3-Methyltriaz-1-ene-1,3-diyl]dibenzonitrile
CAS No.:30091-19-1
Molecular Formula:C15H11 N5
Molecular Weight:261.2813
Hs Code.:
NSC Number:135749
DSSTox Substance ID:DTXSID70300266

Synonyms:30091-19-1;4,4'-[(1e)-3-methyltriaz-1-ene-1,3-diyl]dibenzonitrile;NSC135749;DTXSID70300266;NSC-135749

Suppliers and Price of 4,4'-[(1e)-3-Methyltriaz-1-ene-1,3-diyl]dibenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4,4'-[(1e)-3-Methyltriaz-1-ene-1,3-diyl]dibenzonitrile

Chemical Property:

Boiling Point:465.3°Cat760mmHg
Flash Point:235.2°C
Density:1.13g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:261.10144537
Heavy Atom Count:20
Complexity:424

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=C(C=C1)C#N)N=NC2=CC=C(C=C2)C#N

Technology Process of 4,4'-[(1e)-3-Methyltriaz-1-ene-1,3-diyl]dibenzonitrile

There total 3 articles about 4,4'-[(1e)-3-Methyltriaz-1-ene-1,3-diyl]dibenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 27373-59-7,63193-66-8
1,3-bis(4-cyanophenyl)triazene

: 74-88-4
methyl iodide

: 30091-19-1
1,3-Di-(p-cyanophenyl)-1-methyltriazen

Guidance literature:: With sodium methylate; In methanol; for 26h; Ambient temperature;
DOI:10.1021/jo9703820

Reference yield:

: 873-74-5
4-Aminobenzonitrile

: 30091-19-1
1,3-Di-(p-cyanophenyl)-1-methyltriazen

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / SHNC / H₂O / 18 h / Ambient temperature

2: 92 percent / MeONa / methanol / 26 h / Ambient temperature

With sodium methylate; In methanol; water;
DOI:10.1021/jo9703820