Methanimidamide,N,N'-bis[3-(trifluoromethyl)phenyl]-

Base Information

• Chemical Name: Methanimidamide,N,N'-bis[3-(trifluoromethyl)phenyl]-
• CAS No.: 16659-14-6
• Molecular Formula: C₁₅H₁₀F₆N₂
• Molecular Weight: 332.248
• Mol file: 16659-14-6.mol

Synonyms:Formamidine,N,N'-bis(a,a,a-trifluoro-m-tolyl)- (8CI); N,N'-Di(m-trifluoromethylphenyl)formamidine

Chemical Property of Methanimidamide,N,N'-bis[3-(trifluoromethyl)phenyl]-

Chemical Property:

• Boiling Point: 340.1°Cat760mmHg
• Flash Point: 159.5°C
• Density: 1.3g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanimidamide,N,N'-bis[3-(trifluoromethyl)phenyl]-

There total 1 articles about Methanimidamide,N,N'-bis[3-(trifluoromethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N,N'-bis(m-(trifluoromethyl)phenyl)formamidine (16659-14-6)

Guidance literature:

3-Trifluormethyl-anilin, Orthoameisensaeure-ethylester in abs. Ethanol, (Siedetemp.; 30min);

Reference yield: 88.0%

dirhenium(III) dichlorotetra-μ-acetate (33612-87-2,14126-96-6,15628-76-9) + N,N'-bis(m-(trifluoromethyl)phenyl)formamidine (16659-14-6) → Re2Cl2((CF3)C6H4NCHNC6H4(CF3))4 (253310-86-0)

Guidance literature:

In melt; Ar atmosphere, 156°C (15 h); addn. of EtOH acetate to the hot mixture, stirring (1 h), filtration, washing (EtOH, hexanes), drying (vacuum);

DOI:10.1002/(sici)1099-0682(199911)1999:11<2095::aid-ejic2095>3.0.co;2-t

Reference yield: 65.0%

N,N'-bis(m-(trifluoromethyl)phenyl)formamidine (16659-14-6) + 3-(dicyanomethylidene)-2,3-dihydrobenzothiophene-1,1-dioxide (74228-25-4) → 4-Cyan-3-(3-trifluormethyl-phenylamino)-benzo<4,5>thieno<2,3-c>pyridin-9,9-dioxid (130685-66-4)

Guidance literature:

In chloroform; Heating;

DOI:10.1007/BF00808932

Downstream raw materials:

4-Cyan-3-(3-trifluormethyl-phenylamino)-benzo<4,5>thieno<2,3-c>pyridin-9,9-dioxid

2-(3-Trifluormethyl-anilinomethylen)-2,3-dihydro-3-oxo-benzo-thiophen-1,1-dioxid

2-(3-Trifluormethyl-anilinomethylen)-2,3-dihydro-3-oxo-benzo-thiophen-1,1-dioxid

Re₂Cl₂((CF₃)C₆H₄NCHNC₆H₄(CF₃))4

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