[3aS,4S,6aR,(+)]-Hexahydro-2-oxo-1H-thieno[3,4-d]imidazole-4-pentanoic acid 5-oxide

Base Information

• Chemical Name: [3aS,4S,6aR,(+)]-Hexahydro-2-oxo-1H-thieno[3,4-d]imidazole-4-pentanoic acid 5-oxide
• CAS No.: 3376-83-8
• Molecular Formula: C10H16N2O4S
• Molecular Weight: 260.314
• Mol file: 3376-83-8.mol

Synonyms:biotin N-hydroxysuccinimide ester;Biotin-OSu;D-biotin-N-hydroxysuccinimide ester;N-hydroxysuccinimide-biotin;Biotin-L-sulfoxid;BNHS;d-Biotin NHS ester;d-biotin-d-sulfoxide;N-hydroxysuccinimido biotin;Biotinyl-N-hydroxy-succinimide;N-Succinimidyl D-biotinate;

Chemical Property of [3aS,4S,6aR,(+)]-Hexahydro-2-oxo-1H-thieno[3,4-d]imidazole-4-pentanoic acid 5-oxide

Chemical Property:

• Melting Point: 239-243℃
• Boiling Point: 697°Cat760mmHg
• PKA: 4.72±0.10(Predicted)
• Flash Point: 375.3°C
• PSA: 118.20000
• Density: 1.47g/cm³
• LogP: 0.64680
• Storage Temp.: 2-8°C
• Solubility.: Aqueous Base (Slightly), DMSO (Slightly, Heated)

Purity/Quality:

99%, ^*data from raw suppliers

Biotinsulfoxide 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [3aS,4S,6aR,(+)]-Hexahydro-2-oxo-1H-thieno[3,4-d]imidazole-4-pentanoic acid 5-oxide

There total 3 articles about [3aS,4S,6aR,(+)]-Hexahydro-2-oxo-1H-thieno[3,4-d]imidazole-4-pentanoic acid 5-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ d-biotin l-(S-oxide) (3376-83-8) + d-biotin d-(S-oxide) (10406-89-0)

Guidance literature:

With dihydrogen peroxide; acetic acid;

Reference yield:

biotin (58-85-5,22879-79-4) → d-biotin l-(S-oxide) (3376-83-8)

Guidance literature:

With N-Bromosuccinimide; phosphate buffer;

DOI:10.1021/ja00498a034

Reference yield:

phosgene (75-44-5) → d-biotin l-(S-oxide) (3376-83-8)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

biotin

phosgene

Downstream raw materials:

biotin

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