6-Methyl(1,3)dioxolo(4,5-g)quinolin-8-yl hydrosulfide

Base Information

• Chemical Name: 6-Methyl(1,3)dioxolo(4,5-g)quinolin-8-yl hydrosulfide
• CAS No.: 91918-89-7
• Molecular Formula: C₁₁H₉NO₂S
• Molecular Weight: 219.264
• NSC Number: 332382
• UNII: AK4VC2XJK7
• DSSTox Substance ID: DTXSID80238788
• Mol file: 91918-89-7.mol

Synonyms:91918-89-7;AK4VC2XJK7;6-Methyl(1,3)dioxolo(4,5-g)quinolin-8-yl hydrosulfide;UNII-AK4VC2XJK7;NSC332382;NSC 332382;NSC-332382;6-Methyl[1,3]dioxolo[4,5-g]quinolin-8-yl hydrosulfide;DTXSID80238788;6-Methyl[1,3]dioxolo[4,5-g]quinoline-8-thiol;6-methyl-[1,3]dioxolo[4,5-g]quinoline-8-thiol;6-METHYL-1,3-DIOXOLO(4,5-G)QUINOLINE-8-THIOL;1,3-DIOXOLO(4,5-G)QUINOLINE-8-THIOL, 6-METHYL-

Chemical Property of 6-Methyl(1,3)dioxolo(4,5-g)quinolin-8-yl hydrosulfide

Chemical Property:

• Vapor Pressure: 0.000191mmHg at 25°C
• Boiling Point: 328.3°Cat760mmHg
• Flash Point: 152.4°C
• Density: 1.44g/cm³
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 219.03539970
• Heavy Atom Count: 15
• Complexity: 329

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=S)C2=CC3=C(C=C2N1)OCO3

Technology Process of 6-Methyl(1,3)dioxolo(4,5-g)quinolin-8-yl hydrosulfide

There total 4 articles about 6-Methyl(1,3)dioxolo(4,5-g)quinolin-8-yl hydrosulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-metil-8-cloro-1,3-diossol<4,5-g>chinolina (50593-65-2) → 6-metil-8-mercapto-1,3-diossol<4,5-g>chinolina (91918-89-7)

Guidance literature:

With potassium hydroxide; hydrogen sulfide; In ethanol; for 4h;

Reference yield:

benzo[1,3]dioxolo-5-ylamine (14268-66-7) → 6-metil-8-mercapto-1,3-diossol<4,5-g>chinolina (91918-89-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 48 h / Heating

2: neat (no solvent) / 0.33 h

3: POCl₃ / neat (no solvent) / 1 h / 170 °C

4: KOH, H₂S / ethanol / 4 h

With potassium hydroxide; hydrogen sulfide; trichlorophosphate; In ethanol;

Reference yield:

β-(3,4-metilendiossifenilammino)crotonato di etile (91918-88-6) → 6-metil-8-mercapto-1,3-diossol<4,5-g>chinolina (91918-89-7)

Guidance literature:

Multi-step reaction with 3 steps

1: neat (no solvent) / 0.33 h

2: POCl₃ / neat (no solvent) / 1 h / 170 °C

3: KOH, H₂S / ethanol / 4 h

With potassium hydroxide; hydrogen sulfide; trichlorophosphate; In ethanol;

upstream raw materials:

6-metil-8-cloro-1,3-diossol<4,5-g>chinolina

benzo[1,3]dioxolo-5-ylamine

β-(3,4-metilendiossifenilammino)crotonato di etile

6-metil-8-ossi-1,3-diossol<4,5-g>chinolina