Technology Process of Chlorflavonin
There total 8 articles about Chlorflavonin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) triethylamine; 2.) 60 percent KOH / 1.) 175 deg C, 1 h; 2.) methanol, 30 min, reflux
2: 20 percent / KOH, K2S2O8 / H2O / 12 h
3: 62 percent / K2CO3 / acetone / 1 h / Heating
4: 75 percent / H2 / Pd/C / acetone
With
potassium hydroxide; dipotassium peroxodisulfate; hydrogen; potassium carbonate; triethylamine;
palladium on activated charcoal;
In
water; acetone;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 66.6 percent / K2CO3 / dimethylformamide / 1 h / Heating
2: 84 percent / silver nitrate, 40 percent NaOH / H2O / 0.5 h / Heating
3: 73 percent / pyridine, thionyl chloride / benzene / 14 h
4: 1.) triethylamine; 2.) 60 percent KOH / 1.) 175 deg C, 1 h; 2.) methanol, 30 min, reflux
5: 20 percent / KOH, K2S2O8 / H2O / 12 h
6: 62 percent / K2CO3 / acetone / 1 h / Heating
7: 75 percent / H2 / Pd/C / acetone
With
pyridine; potassium hydroxide; sodium hydroxide; dipotassium peroxodisulfate; thionyl chloride; hydrogen; potassium carbonate; silver nitrate; triethylamine;
palladium on activated charcoal;
In
water; N,N-dimethyl-formamide; acetone; benzene;
