(4Z)-4-({[4-(4-chlorophenyl)piperazin-1-yl]amino}methylidene)-2-methoxycyclohexa-2,5-dien-1-one

Base Information

• Chemical Name: (4Z)-4-({[4-(4-chlorophenyl)piperazin-1-yl]amino}methylidene)-2-methoxycyclohexa-2,5-dien-1-one
• CAS No.: 5784-08-7
• Molecular Formula: C18H20ClN3O2
• Molecular Weight: 171.283
• Mol file: 5784-08-7.mol

Synonyms:

Chemical Property of (4Z)-4-({[4-(4-chlorophenyl)piperazin-1-yl]amino}methylidene)-2-methoxycyclohexa-2,5-dien-1-one

Chemical Property:

• Vapor Pressure: 4.59E-11mmHg at 25°C
• Boiling Point: 523.7°Cat760mmHg
• Flash Point: 270.6°C
• Density: 1.31g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4Z)-4-({[4-(4-chlorophenyl)piperazin-1-yl]amino}methylidene)-2-methoxycyclohexa-2,5-dien-1-one

There total 5 articles about (4Z)-4-({[4-(4-chlorophenyl)piperazin-1-yl]amino}methylidene)-2-methoxycyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

1-aminodecane (2016-57-1) + acetone (67-64-1) → 1-decanal oxime (5780-38-1) + (E)-decanaloxime (5784-08-7) + 2-Decyl-3,3-dimethyloxaziridine (144348-00-5) + 1-nitrosodecane dimer (99729-93-8)

Guidance literature:

With potassium sulfate; potassium hydrogensulfate; potassium peroxomonosulfate; sodium hydrogencarbonate; In dichloromethane; water; Yields of byproduct given;

DOI:10.1021/jo00051a017

Reference yield:

caprinaldehyde (112-31-2) → 1-decanal oxime (5780-38-1) + (E)-decanaloxime (5784-08-7)

Guidance literature:

With iron(II) perchlorate hexahydrate; ethyl acetohydroximate; In dichloromethane; at 20 ℃; for 24h; Reagent/catalyst; Solvent; Overall yield = 98 %; Inert atmosphere;

Reference yield:

caprinaldehyde (112-31-2) → (E)-decanaloxime (5784-08-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; In water; at 20 ℃;

DOI:10.1002/cmdc.200900418

upstream raw materials:

1-aminodecane

acetone

caprinaldehyde

Downstream raw materials:

n-decanenitrile

N-decylhydroxyl-amine