1,3,5-TRIFLUORO-2,4,6-TRIMETHYLBENZENE

Base Information

• Chemical Name: 1,3,5-TRIFLUORO-2,4,6-TRIMETHYLBENZENE
• CAS No.: 363-64-4
• Molecular Formula: C9H9 F3
• Molecular Weight: 174.166
• Hs Code.: 2903999090
• Mol file: 363-64-4.mol

Synonyms:Mesitylene,2,4,6-trifluoro- (8CI); 2,4,6-Trifluoromesitylene; NSC 10356

Chemical Property of 1,3,5-TRIFLUORO-2,4,6-TRIMETHYLBENZENE

Chemical Property:

• Vapor Pressure: 0.0075mmHg at 25°C
• Melting Point: 67-68
• Boiling Point: 168-169
• Flash Point: 50.9°C
• PSA: 0.00000
• Density: 1.154g/cm³
• LogP: 3.02910

Purity/Quality:

98%min ^*data from raw suppliers

1,3,5-TRIFLUORO-2,4,6-TRIMETHYLBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,5-TRIFLUORO-2,4,6-TRIMETHYLBENZENE

There total 7 articles about 1,3,5-TRIFLUORO-2,4,6-TRIMETHYLBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-difluoro-2,4,6-trimethyl-aniline (443-98-1) → 1,3,5-trimethyl-2,4,6-trifluorobenzene (363-64-4)

Guidance literature:

With hydrogenchloride; sodium tetrafluoroborate; sodium nitrite; Erhitzen des Reaktionsprodukts;

DOI:10.1021/ja01145a055

Reference yield:

2-fluoro-1,3,5-trimethyl-4-nitro-benzene (386-66-3) → 1,3,5-trimethyl-2,4,6-trifluorobenzene (363-64-4)

Guidance literature:

Multi-step reaction with 5 steps

1: iron

2: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts

3: hydrogen fluoride; sodium nitrate

4: iron

5: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts

With hydrogenchloride; sodium nitrate; sodium tetrafluoroborate; hydrogen fluoride; iron; sodium nitrite;

DOI:10.1021/ja01145a055

Reference yield:

1,3-difluoro-2,4,6-trimethylbenzene (392-61-0) → 1,3,5-trimethyl-2,4,6-trifluorobenzene (363-64-4)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen fluoride; sodium nitrate

2: iron

3: aqueous hydrochloric acid; sodium nitrite; aqueous sodium fluoroborate solution / Erhitzen des Reaktionsprodukts

With hydrogenchloride; sodium nitrate; sodium tetrafluoroborate; hydrogen fluoride; iron; sodium nitrite;

DOI:10.1021/ja01145a055

upstream raw materials:

3,5-difluoro-2,4,6-trimethyl-aniline

1,3,5-trifluorobenzene

methyl iodide

2-fluoro-1,3,5-trimethyl-4-nitro-benzene

Downstream raw materials:

1,3,5-tris-dichloromethyl-2,4,6-trifluoro-benzene

1,3,5-trifluoro-2,4,6-tris-trichloromethyl-benzene

1,3,5-trichlorotrifluorobenzene

Refernces