n-Nitroso-n-phenylacetamide

Base Information

• Chemical Name: n-Nitroso-n-phenylacetamide
• CAS No.: 938-81-8
• Molecular Formula: C8H8N2O2
• Molecular Weight: 164.164
• Hs Code.: 2924299090
• NSC Number: 95272
• DSSTox Substance ID: DTXSID20294227
• Nikkaji Number: J80.034A
• Wikidata: Q82033407
• Mol file: 938-81-8.mol

Synonyms:n-nitroso-n-phenylacetamide;938-81-8;N-NITROSOACETANILIDE;NSC95272;SCHEMBL4365636;DTXSID20294227;NSC-95272

Chemical Property of n-Nitroso-n-phenylacetamide

Chemical Property:

• Vapor Pressure: 0.0361mmHg at 25°C
• Melting Point: 51°C (rough estimate)
• Refractive Index: 1.6000 (estimate)
• Boiling Point: 241.3°Cat760mmHg
• Flash Point: 99.7°C
• PSA: 49.74000
• Density: 1.15g/cm³
• LogP: 1.72090
• XLogP3: 1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 164.058577502
• Heavy Atom Count: 12
• Complexity: 176

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)N(C1=CC=CC=C1)N=O
• Uses: N-Nitroso Acetanilide is a synthesis intermediate, a nitric oxide-donor, and an oxidizer in radical processes.

Technology Process of n-Nitroso-n-phenylacetamide

There total 5 articles about n-Nitroso-n-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

Acetanilid (103-84-4) → N-nitrosoacetanilide (938-81-8)

Guidance literature:

With acetic anhydride; sodium nitrite; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

cis-nitrous acid (7782-77-6) + Acetanilid (103-84-4) → N-nitrosoacetanilide (938-81-8)

Guidance literature:

In acetic acid;

Reference yield:

benzenediazonium (2684-02-8) + acetic anhydride (108-24-7) → N-nitrosoacetanilide (938-81-8)

Guidance literature:

With alkali;

upstream raw materials:

benzenediazonium

acetic anhydride

Acetanilid

cis-nitrous acid

Downstream raw materials:

benzene

2-phenylthiophene

3-phenylthiophene

(E)-1-methyl-2-(phenyldiazenyl)-1H-pyrrole