Technology Process of Cyclohexanemethanamine, alpha-methyl-4-phenyl-, trans-
There total 4 articles about Cyclohexanemethanamine, alpha-methyl-4-phenyl-, trans- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 76 percent / hydroxylamine hydrochloride, NaOH / ethanol; H2O / 5 h / Heating
2: 1.) LiAlH4; 2.) 15percent NaOH / 1.) ether, THF, reflux, 11 h; 2.) water, 0.5 h, r.t.
With
sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride;
In
ethanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) Li / 1.) ether, 1 h, r.t; 2.) ether, reflux, 8 h
2: 76 percent / hydroxylamine hydrochloride, NaOH / ethanol; H2O / 5 h / Heating
3: 1.) LiAlH4; 2.) 15percent NaOH / 1.) ether, THF, reflux, 11 h; 2.) water, 0.5 h, r.t.
With
sodium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; lithium;
In
ethanol; water;
- Guidance literature:
-
With
sodium hydroxide; lithium aluminium tetrahydride;
Yield given. Multistep reaction;
1.) ether, THF, reflux, 11 h; 2.) water, 0.5 h, r.t.;
