2-(Biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

Base Information

Chemical Name:2-(Biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate
CAS No.:4347-68-6
Molecular Formula:C21H15BrO3
Molecular Weight:395.246
Hs Code.:
NSC Number:115843
DSSTox Substance ID:DTXSID50297403
Wikidata:Q82038477

Synonyms:4347-68-6;2-(biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate;NSC115843;Oprea1_405876;DTXSID50297403;NSC-115843

Suppliers and Price of 2-(Biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-(Biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

Chemical Property:

Vapor Pressure:4.74E-12mmHg at 25°C
Boiling Point:547.7°Cat760mmHg
Flash Point:285.1°C
Density:1.388g/cm³
XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:394.02046
Heavy Atom Count:25
Complexity:450

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC=C(C=C2)C(=O)COC(=O)C3=CC=CC=C3Br

Technology Process of 2-(Biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

There total 4 articles about 2-(Biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 135-73-9
2-Bromo-4'-phenylacetophenone

: 88-65-3
2-bromobenzoic-acid

: 4347-68-6
2-(biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

Guidance literature:: 2-bromobenzoic-acid; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

2-Bromo-4'-phenylacetophenone; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.ijbiomac.2020.11.170

Reference yield:

: 92-91-1
biphenyl-4-acetaldehyde

: 4347-68-6
2-(biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; bromine / 45 - 50 °C

With bromine; acetic acid;
DOI:10.1021/ja01344a056

Reference yield:

: 92-52-4,1594-86-1
biphenyl

: 4347-68-6
2-(biphenyl-4-yl)-2-oxoethyl 2-bromobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃; carbon disulfide

2: acetic acid; bromine / 45 - 50 °C

With carbon disulfide; aluminium trichloride; bromine; acetic acid;
DOI:10.1021/ja01344a056