6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro-[8,8'-biisoquinoline]-7,7'-diol

Base Information

• Chemical Name: 6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro-[8,8'-biisoquinoline]-7,7'-diol
• CAS No.: 14510-48-6
• Molecular Formula: C₂₂H₂₈N₂O₄
• Molecular Weight: 384.475
• NSC Number: 131725
• DSSTox Substance ID: DTXSID50299644
• Wikidata: Q82042143
• Mol file: 14510-48-6.mol

Synonyms:14510-48-6;6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro-[8,8'-biisoquinoline]-7,7'-diol;NSC131725;DTXSID50299644;NSC-131725;6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro[8,8'-biisoquinoline]-7,7'-diol

Chemical Property of 6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro-[8,8'-biisoquinoline]-7,7'-diol

Chemical Property:

• Boiling Point: 550°Cat760mmHg
• Flash Point: 286.5°C
• Density: 1.219g/cm³
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 384.20490738
• Heavy Atom Count: 28
• Complexity: 489

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1CCC2=CC(=C(C(=C2C1)C3=C4CN(CCC4=CC(=C3O)OC)C)O)OC

Technology Process of 6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro-[8,8'-biisoquinoline]-7,7'-diol

There total 1 articles about 6,6'-Dimethoxy-2,2'-dimethyl-1,1',2,2',3,3',4,4'-octahydro-[8,8'-biisoquinoline]-7,7'-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

6-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinolin-7-ol (450-14-6) + 1-phenyl-p-quinol acetate (35006-00-9) → 6-methoxy-2-methyl-1-phenyl-1,2,3,4-tetrahydro-isoquinolin-7-ol (4667-10-1) + corypalline dimer (14510-48-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 1h; Ambient temperature;

upstream raw materials:

6-methoxy-2-methyl-1,2,3,4-tetrahydro-isoquinolin-7-ol

1-phenyl-p-quinol acetate

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