Diethyl 2-Oxo-1,2-dihydro-4,5-pyriMidinedicarboxylate

Base Information

• Chemical Name: Diethyl 2-Oxo-1,2-dihydro-4,5-pyriMidinedicarboxylate
• CAS No.: 62328-19-2
• Molecular Formula: C10H12N2O5
• Molecular Weight: 240.2127
• Hs Code.: 2933599090
• Mol file: 62328-19-2.mol

Synonyms:diethyl 2-hydroxypyrimidine-4,5-dicarboxylate;2-oxo-1(3),2-dihydro-pyrimidine-4,5-dicarboxylic acid diethyl ester;2-Hydroxy-4,5-diethoxycarbonyl-pyrimidin;2-Hydroxy-pyrimidin-4,5-dicarbonsaeurediethylester;Diethyl2-Oxo-1,2-dihydro-4,5-pyrimidinedicarboxylate;DIETHYL 2-OXO-3H-PYRIMIDINE-4,5-DICARBOXYLATE;

Chemical Property of Diethyl 2-Oxo-1,2-dihydro-4,5-pyriMidinedicarboxylate

Chemical Property:

• Vapor Pressure: 5.57E-07mmHg at 25°C
• Boiling Point: 400.3°Cat760mmHg
• Flash Point: 195.9°C
• PSA: 98.61000
• Density: 1.35g/cm³
• LogP: 0.53560
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Diethyl2-oxo-1,2-dihydropyrimidine-4,5-dicarboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Diethyl 2-Oxo-1,2-dihydro-4,5-pyriMidinedicarboxylate

There total 5 articles about Diethyl 2-Oxo-1,2-dihydro-4,5-pyriMidinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

→ 2-Hydroxy-4,5-diethoxycarbonyl-pyrimidin (62328-19-2)

Guidance literature:

Reference yield:

ureidomethylen-oxalacetic acid diethyl ester → 2-oxo-1,2-dihydro-pyrimidine-4,5-dicarboxylic acid diethyl ester (62328-19-2)

Guidance literature:

With xylene;

DOI:10.1021/jo01127a008

Reference yield:

diethyl(ethoxymethylene)oxalacetate (52942-64-0,55130-49-9) → 2-oxo-1,2-dihydro-pyrimidine-4,5-dicarboxylic acid diethyl ester (62328-19-2)

Guidance literature:

Multi-step reaction with 2 steps

2: xylene

With xylene;

DOI:10.1021/jo01127a008

upstream raw materials:

orthoformic acid triethyl ester

urea

diethyl oxaloacetate

diethyl(ethoxymethylene)oxalacetate