2,7-Octadienal, 2-methyl-6-methylene-, (E)-

Base Information

Chemical Name:2,7-Octadienal, 2-methyl-6-methylene-, (E)-
CAS No.:17015-30-4
Molecular Formula:C₁₀H₁₄O
Molecular Weight:150.221
Hs Code.:
Mol file:17015-30-4.mol

Synonyms:2,7-Octadienal, 2-methyl-6-methylene-, (E)-;17015-30-4;SCHEMBL8934689;NDYNCPVWWPJJKN-JXMROGBWSA-N;(e)-2-methyl-6-methylene-2,7-octadienal

Suppliers and Price of 2,7-Octadienal, 2-methyl-6-methylene-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2,7-Octadienal, 2-methyl-6-methylene-, (E)-

Chemical Property:

Vapor Pressure:0.0515mmHg at 25°C
Boiling Point:234.9°C at 760 mmHg
Flash Point:102.9°C
Density:0.861g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:150.104465066
Heavy Atom Count:11
Complexity:187

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCCC(=C)C=C)C=O
Isomeric SMILES:C/C(=C\CCC(=C)C=C)/C=O

Technology Process of 2,7-Octadienal, 2-methyl-6-methylene-, (E)-

There total 11 articles about 2,7-Octadienal, 2-methyl-6-methylene-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26394-25-2
(E)-4-chloro-2-methylbut-2-enal

: 17015-30-4
2-methyl-6-methylene-2,7-octadienal

Guidance literature:: Multi-step reaction with 6 steps

1: 54 percent / p-toluenesulfonic acid / cyclohexane / Heating

2: 1.) NaOCH₃ / 1.) CH₃OH, RT, 0.5 h, 2.) CH₃OH, RT, overnight

3: aq. NaOH / 2 h / 60 °C

4: 1.) Mg / 1.) THF, 2.) THF, 30 deg C, 0.5 h

5: 79 percent / aq. oxalic acid / acetone / 1 h / Ambient temperature

6: KHSO₄ / 180 °C

With sodium hydroxide; potassium hydrogensulfate; sodium methylate; oxalic acid; toluene-4-sulfonic acid; magnesium; In cyclohexane; acetone;
DOI:10.1021/jf00035a047

Reference yield:

: 3330-23-2
2-hydroxy-2-methyl-3-butenal dimethyl acetal

: 17015-30-4
2-methyl-6-methylene-2,7-octadienal

Guidance literature:: Multi-step reaction with 7 steps

1: 43 percent / aq. HCl, NaCl, CuC / toluene / 6 h / 50 °C

2: 54 percent / p-toluenesulfonic acid / cyclohexane / Heating

3: 1.) NaOCH₃ / 1.) CH₃OH, RT, 0.5 h, 2.) CH₃OH, RT, overnight

4: aq. NaOH / 2 h / 60 °C

5: 1.) Mg / 1.) THF, 2.) THF, 30 deg C, 0.5 h

6: 79 percent / aq. oxalic acid / acetone / 1 h / Ambient temperature

7: KHSO₄ / 180 °C

With hydrogenchloride; sodium hydroxide; potassium hydrogensulfate; sodium methylate; oxalic acid; toluene-4-sulfonic acid; magnesium; sodium chloride; In cyclohexane; acetone; toluene;
DOI:10.1021/jf00035a047

Reference yield:

: 118757-23-6
2-methyl-4-chloro-2-butenal ethylene glycol acetal

: 17015-30-4
2-methyl-6-methylene-2,7-octadienal

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaOCH₃ / 1.) CH₃OH, RT, 0.5 h, 2.) CH₃OH, RT, overnight

2: aq. NaOH / 2 h / 60 °C

3: 1.) Mg / 1.) THF, 2.) THF, 30 deg C, 0.5 h

4: 79 percent / aq. oxalic acid / acetone / 1 h / Ambient temperature

5: KHSO₄ / 180 °C

With sodium hydroxide; potassium hydrogensulfate; sodium methylate; oxalic acid; magnesium; In acetone;
DOI:10.1021/jf00035a047