C3Hvf3T92D

Base Information

Chemical Name:C3Hvf3T92D
CAS No.:219566-51-5
Molecular Formula:
Molecular Weight:425.53229
Hs Code.:
UNII:C3HVF3T92D
Nikkaji Number:J1.008.306K
Mol file:219566-51-5.mol

Synonyms:C3HVF3T92D;FR-119680;UNII-C3HVF3T92D;FR119680;1-((6,6-Dimethyl-6H-dibenzo(b,d)pyran-3-yl)methyl)-1H-indole-3-butanoic acid;1H-Indole-3-butanoic acid, 1-((6,6-dimethyl-6H-dibenzo(b,d)pyran-3-yl)methyl)-;4-(1-((6,6-Dimethyl-6H-benzo(C)chromen-3-yl)methyl)-1H-indol-3-yl)butanoic acid;219566-51-5

Suppliers and Price of C3Hvf3T92D

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C3Hvf3T92D

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:425.19909372
Heavy Atom Count:32
Complexity:663

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(C2=CC=CC=C2C3=C(O1)C=C(C=C3)CN4C=C(C5=CC=CC=C54)CCCC(=O)O)C

Technology Process of C3Hvf3T92D

There total 3 articles about C3Hvf3T92D which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 219544-46-4
3,6,6-trimethyl-7,8,9,10-tetrahydro-6H-dibenzopyran

: 219566-51-5
4-<1-(6,6-dimethyl-6H-dibenzopyran-3-yl)methyl-indol-3-yl>butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 94.1 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / toluene / 4 h / Heating

2: 48.8 percent / N-bromosuccinimide, 2,2'-azobis(4-methoxy-2,4-dimethylvaleronitrile) / CCl₄ / 1.5 h / Heating

3: 1.) NaH / 1.) DMF, 20 deg C, 30 min, 2.) DMF, 20 deg C, 1 h

With N-Bromosuccinimide; 2,2’-azobis(4-methoxy-2,4-dimethyl)valeronitrile; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrachloromethane; toluene;
DOI:10.1248/cpb.46.1683

Reference yield:

: 219544-48-6
3,6,6-trimethyl-6H-dibenzopyran

: 219566-51-5
4-<1-(6,6-dimethyl-6H-dibenzopyran-3-yl)methyl-indol-3-yl>butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 48.8 percent / N-bromosuccinimide, 2,2'-azobis(4-methoxy-2,4-dimethylvaleronitrile) / CCl₄ / 1.5 h / Heating

2: 1.) NaH / 1.) DMF, 20 deg C, 30 min, 2.) DMF, 20 deg C, 1 h

With N-Bromosuccinimide; 2,2’-azobis(4-methoxy-2,4-dimethyl)valeronitrile; sodium hydride; In tetrachloromethane;
DOI:10.1248/cpb.46.1683

Reference yield:

: 133-32-4
4-indol-3-yl-butyric acid

: 219544-50-0
3-(bromomethyl)-6,6-dimethyl-6H-dibenzopyran-6-one

: 219566-51-5
4-<1-(6,6-dimethyl-6H-dibenzopyran-3-yl)methyl-indol-3-yl>butyric acid

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) DMF, 20 deg C, 30 min, 2.) DMF, 20 deg C, 1 h;
DOI:10.1248/cpb.46.1683