trimethyl (phosphoryltrimethanediyl)triscarbamate

Base Information

• Chemical Name: trimethyl (phosphoryltrimethanediyl)triscarbamate
• CAS No.: 63833-13-6
• Molecular Formula: C9H18 N3 O7 P
• Molecular Weight: 311.232
• Mol file: 63833-13-6.mol

Synonyms:2-Oxa-4,8-diaza-6-phosphanonan-9-oicacid, 6-[[(methoxycarbonyl)amino]methyl]-3-oxo-, methyl ester, 6-oxide (9CI);NSC 299162; Tris[N-(methoxycarbonyl)aminomethyl]phosphine oxide

Chemical Property of trimethyl (phosphoryltrimethanediyl)triscarbamate

Chemical Property:

• Vapor Pressure: 7.05E-14mmHg at 25°C
• Boiling Point: 589.6°Cat760mmHg
• Flash Point: 310.4°C
• Density: 1.306g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trimethyl (phosphoryltrimethanediyl)triscarbamate

There total 5 articles about trimethyl (phosphoryltrimethanediyl)triscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(CH3 O2 CNHCH2)3 P + tris(N-carbomethoxylaminomethyl)phosphine (63833-12-5) → tris(N-carbomethoxylaminomethyl)phosphine oxide (63833-13-6)

Guidance literature:

With dihydrogen peroxide; In acetone;

Reference yield: 73.0%

octakis(N-carbomethoxylaminomethyl)diphosphonium sulfate (77350-09-5) → tris(N-carbomethoxylaminomethyl)phosphine oxide (63833-13-6)

Guidance literature:

With ammonium hydroxide; In water; for 0.0833333h; Ambient temperature;

Reference yield: 53.1%

tris(N-carbomethoxylaminomethyl)phosphine (63833-12-5) → tris(N-carbomethoxylaminomethyl)phosphine oxide (63833-13-6)

Guidance literature:

With dihydrogen peroxide; In water; at 20 - 30 ℃; for 3.5h;

upstream raw materials:

tris(N-carbomethoxylaminomethyl)phosphine

octakis(N-carbomethoxylaminomethyl)diphosphonium sulfate

tris(aminomethyl)phosphine oxide

methyl chloroformate

Downstream raw materials:

methyl iodide

tris(aminomethyl)phosphine oxide

5-aminomethyl-1,3-diaza-5-phosphorinan-2,5-dione

methylene chloride