3-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-ylidene)-2,N,N-trimethyl-1-propanamine

Base Information

Chemical Name:3-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-ylidene)-2,N,N-trimethyl-1-propanamine
CAS No.:67195-26-0
Molecular Formula:C21H25N
Molecular Weight:291.43
Hs Code.:
Mol file:67195-26-0.mol

Synonyms:3-(10,11-dihydro-5H-dibenzo[a,d][7]annulen-5-ylidene)-N,N,2-trimethylpropan-1-amine;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-ylidene)-2,N,N-trimethyl-1-propanamine

Chemical Property:

Vapor Pressure:7.73E-07mmHg at 25°C
Boiling Point:407.1°C at 760 mmHg
Flash Point:178.4°C
PSA：3.24000
Density:1.06g/cm³
LogP:4.41460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-ylidene)-2,N,N-trimethyl-1-propanamine

There total 4 articles about 3-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-ylidene)-2,N,N-trimethyl-1-propanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2625-17-4
rac.-5-Hydroxy-5-<3-dimethylamino-2-methyl-propyl>-dibenzo<1,4>cycloheptadien

: 67195-26-0
rac.-5-<3-Dimethylamino-2-methyl-propyliden>-dibenzo<1,4>cycloheptadien

Guidance literature:: With acetic anhydride; Heating;
DOI:10.1021/jo01048a057

Reference yield:

: 1210-35-1
10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

: 67195-26-0
rac.-5-<3-Dimethylamino-2-methyl-propyliden>-dibenzo<1,4>cycloheptadien

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Mg, (ii) /BRN= 1454355/, THF

2: Ac₂O / Heating

With acetic anhydride;
DOI:10.1021/jo01048a057

Reference yield:

: 23349-86-2
3-(dimethylamino)-2-methylpropylchloride

: 67195-26-0
rac.-5-<3-Dimethylamino-2-methyl-propyliden>-dibenzo<1,4>cycloheptadien

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Mg, (ii) /BRN= 1454355/, THF

2: Ac₂O / Heating

With acetic anhydride;
DOI:10.1021/jo01048a057