3-(butylamino)-4-chloro-5-sulfamoylbenzoic acid

Base Information

Chemical Name:3-(butylamino)-4-chloro-5-sulfamoylbenzoic acid
CAS No.:22893-29-4
Molecular Formula:C11H15 Cl N2 O4 S
Molecular Weight:306.77
Hs Code.:
Mol file:22893-29-4.mol

Synonyms:Benzoicacid, 3-(butylamino)-4-chloro-5-sulfamoyl- (8CI);3-(Butylamino)-4-chloro-5-sulfamoylbenzoic acid;3-n-Butylamino-4-chloro-5-sulfamoylbenzoic acid; HH 594

Suppliers and Price of 3-(butylamino)-4-chloro-5-sulfamoylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 3-(butylamino)-4-chloro-5-sulfamoylbenzoic acid

Chemical Property:

Vapor Pressure:1.31E-13mmHg at 25°C
Boiling Point:565.1°Cat760mmHg
Flash Point:295.6°C
Density:1.448g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(butylamino)-4-chloro-5-sulfamoylbenzoic acid

There total 6 articles about 3-(butylamino)-4-chloro-5-sulfamoylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1357465-09-8
3-butylamino-4-chloro-5-(dimethylaminomethylene-sulfamoyl)-benzoic acid methyl ester

: 22893-29-4
3-butylamino-4-chloro-5-sulfamoyl-benzoic acid

Guidance literature:: 3-butylamino-4-chloro-5-(dimethylaminomethylene-sulfamoyl)-benzoic acid methyl ester; With water; sodium hydroxide; In methanol; at 50 ℃; for 2h;

With hydrogenchloride; In water;

Reference yield:

: 22892-96-2
4-chloro-3-nitro-5-sulfamoylbenzoic acid

: 22893-29-4
3-butylamino-4-chloro-5-sulfamoyl-benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / 50 °C

2: acetonitrile / 20 °C

3: water; ammonium chloride; iron / ethanol / 2.05 h / 85 °C

4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C

5: borane-THF / tetrahydrofuran / 1 h / 20 °C

6: sodium hydroxide; water / methanol / 2 h / 50 °C

With thionyl chloride; borane-THF; water; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; acetonitrile;

Reference yield:

: 67155-14-0
4-chloro-3-nitro-5-sulfamoyl-benzoic acid methyl ester

: 22893-29-4
3-butylamino-4-chloro-5-sulfamoyl-benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: acetonitrile / 20 °C

2: water; ammonium chloride; iron / ethanol / 2.05 h / 85 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C

4: borane-THF / tetrahydrofuran / 1 h / 20 °C

5: sodium hydroxide; water / methanol / 2 h / 50 °C

With borane-THF; water; iron; ammonium chloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; acetonitrile;