N,N-Diethyl-2,4-dimethylbenzamide

Base Information

Chemical Name:N,N-Diethyl-2,4-dimethylbenzamide
CAS No.:54818-95-0
Molecular Formula:C13H19NO
Molecular Weight:205.3
Hs Code.:2924299090
DSSTox Substance ID:DTXSID60203318
Nikkaji Number:J149.097D
Wikidata:Q83076682
ChEMBL ID:CHEMBL4932325
Mol file:54818-95-0.mol

Synonyms:N,N-Diethyl-2,4-dimethylbenzamide;DEXA;54818-95-0;BENZAMIDE, N,N-DIETHYL-2,4-DIMETHYL-;BRN 2099453;SCHEMBL509845;CHEMBL4932325;DTXSID60203318;AKOS008930266;CCG-345328;LS-26471;Z31723533

Suppliers and Price of N,N-Diethyl-2,4-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N,N-DIETHYL-2,4-DIMETHYLBENZAMIDE 95.00%
5MG
$ 500.43

Total 4 raw suppliers

Chemical Property of N,N-Diethyl-2,4-dimethylbenzamide

Chemical Property:

Vapor Pressure:6.88E-05mmHg at 25°C
Boiling Point:343.8°Cat760mmHg
Flash Point:153.5°C
PSA：20.31000
Density:0.976g/cm³
LogP:2.78540
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:205.146664230
Heavy Atom Count:15
Complexity:211

Purity/Quality:

99% ^*data from raw suppliers

N,N-DIETHYL-2,4-DIMETHYLBENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=C(C=C1)C)C

Technology Process of N,N-Diethyl-2,4-dimethylbenzamide

There total 4 articles about N,N-Diethyl-2,4-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 36598-12-6
bis(N,N-diethylcarbamoyl) diselenide

: 108-38-3,104809-90-7
m-xylene

: 54818-95-0
N,N-diethyl-2,4-dimethyl-benzamide

: 57806-77-6
1-(N,N-diethylcarbamoyl)-2,6-dimethylbenzene

Guidance literature:: With mercury dibromide; In various solvent(s); for 12h; Heating;
DOI:10.1016/S0040-4039(00)82282-0

Reference yield:

: 109-89-7
diethylamine

: 21900-42-5
2,4-dimethylbenzoyl chloride

: 54818-95-0
N,N-diethyl-2,4-dimethyl-benzamide

Guidance literature:: In dichloromethane; at 0 ℃;
DOI:10.1016/j.tet.2009.10.027

Reference yield:

: 611-01-8
2,4-dimethyl-benzoic acid

: 54818-95-0
N,N-diethyl-2,4-dimethyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 0 °C / Reflux; Inert atmosphere

2: dichloromethane / 0 °C / Inert atmosphere

With thionyl chloride; In dichloromethane;
DOI:10.1016/j.tet.2011.10.053