Sodium 9,10-dimethoxyanthracene-2-sulfonate

Base Information

• Chemical Name: Sodium 9,10-dimethoxyanthracene-2-sulfonate
• CAS No.: 67580-39-6
• Molecular Formula: C16H13NaO5S
• Molecular Weight: 340.332
• Hs Code.: 2909309090
• European Community (EC) Number: 266-720-4
• DSSTox Substance ID: DTXSID90986940
• Nikkaji Number: J254.892E
• Mol file: 67580-39-6.mol

Synonyms:Sodium 9,10-dimethoxyanthracene-2-sulfonate;67580-39-6;Sodium 9,10-dimethoxyanthracene-2-sulphonate;9,10-Dimethoxyanthracene-2-sulfonic Acid Sodium Salt;sodium;9,10-dimethoxyanthracene-2-sulfonate;EINECS 266-720-4;9,10-Dimethoxy-2-anthracenesulfonic acid sodium salt;IPA-DAS;C16H14O5S.Na;SCHEMBL2858129;C16-H14-O5-S.Na;DTXSID90986940;CBGQZXMEEWCJQD-UHFFFAOYSA-M;BCP32484;MFCD00042061;AKOS000478987;AKOS015902427;AS-65833;FT-0767348;T71211;9,10-Dimethoxy-2-anthracenesulfonic acid sodium salt, for fluorescence, >=96.0% (HPLC)

Chemical Property of Sodium 9,10-dimethoxyanthracene-2-sulfonate

Chemical Property:

• Melting Point: >200°C (dec.)
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 84.04000
• Density: 1.393g/cm³
• LogP: 3.99510
• Storage Temp.: Hygroscopic, -20°C Freezer, Under inert atmosphere
• Solubility.: DMSO (Slightly), Methanol (Very Slightly)
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 340.03813897
• Heavy Atom Count: 23
• Complexity: 491

Purity/Quality:

98%,99%, ^*data from raw suppliers

9,10-Dimethoxy-2-anthracenesulfonic acid sodium salt ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: COC1=C2C=CC(=CC2=C(C3=CC=CC=C31)OC)S(=O)(=O)[O-].[Na+]
• Uses: ZnAF-1F is a probe for fluorimetric detection of zinc. It can be used in engineering or chemical process and engineered material use in tuning the performance of aqueous photovoltaic elastomer gels by solvent polarity and nanostructure development.

Technology Process of Sodium 9,10-dimethoxyanthracene-2-sulfonate

There total 1 articles about Sodium 9,10-dimethoxyanthracene-2-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium anthraquinone-2-sulfonate (131-08-8) + dimethyl sulfate (77-78-1) → 9,10-dimethoxy-2-anthracenesulfonic acid sodium salt (67580-39-6)

Guidance literature:

With sodium hydroxide; zinc; In ethanol; at 80 ℃;

DOI:10.1039/P29900001709

Reference yield:

9,10-dimethoxy-2-anthracenesulfonic acid sodium salt (67580-39-6) → p-nitrobenzyl 9,10-dimethoxyanthracene-2-sulphonate (121172-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₅ / toluene / 1 h / 40 °C

2: trimethylamine / toluene / 24 h / Ambient temperature

With phosphorus pentachloride; trimethylamine; In toluene;

DOI:10.1039/P29900001709

Reference yield:

diphenyliodonium chloride (1483-72-3) + 9,10-dimethoxy-2-anthracenesulfonic acid sodium salt (67580-39-6) → Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate (137308-86-2)

Guidance literature:

In water; Heating;

DOI:10.1246/cl.1991.1869

upstream raw materials:

sodium anthraquinone-2-sulfonate

dimethyl sulfate

Downstream raw materials:

Diphenyliodonium 9,10-dimethoxyanthracene-2-sulfonate

p-nitrobenzyl 9,10-dimethoxyanthracene-2-sulphonate

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