2-AMINO-N-P-TOLYL-BENZAMIDE

Base Information

• Chemical Name: 2-AMINO-N-P-TOLYL-BENZAMIDE
• CAS No.: 32212-38-7
• Molecular Formula: C14H14 N2 O
• Molecular Weight: 226.278
• Hs Code.: 2924299090
• Mol file: 32212-38-7.mol

Synonyms:p-Benzotoluidide,2-amino- (6CI,7CI,8CI); 2-Amino-N-(4-methylphenyl)benzamide;4-Methylanthranilanilide; NSC 409215

Chemical Property of 2-AMINO-N-P-TOLYL-BENZAMIDE

Chemical Property:

• Vapor Pressure: 0.000229mmHg at 25°C
• Melting Point: 189 °C
• Boiling Point: 325.5°Cat760mmHg
• PKA: 13.25±0.70(Predicted)
• Flash Point: 150.7°C
• PSA: 55.12000
• Density: 1.21g/cm³
• LogP: 3.48370
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-N-(4-methylphenyl)benzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-AMINO-N-P-TOLYL-BENZAMIDE

There total 18 articles about 2-AMINO-N-P-TOLYL-BENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-nitro-N-(4-methylphenyl)benzamide (50623-00-2) → 2-amino-N-(4-methylphenyl)benzamide (32212-38-7)

Guidance literature:

With titanium tetrachloride; zinc; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2007.07.011

Reference yield: 87.0%

isatoic anhydride (118-48-9) + p-toluidine (106-49-0,12221-03-3) → 2-amino-N-(4-methylphenyl)benzamide (32212-38-7)

Guidance literature:

for 0.0333333h; microwave irradiation;

Reference yield: 81.0%

→ 2-amino-N-(4-methylphenyl)benzamide (32212-38-7)

Guidance literature:

With tin(II) chloride hydrate; In ethyl acetate; Reflux;

upstream raw materials:

isatoic anhydride

p-toluidine

diethyl ether

2-(sulfinylamino)benzoyl chloride

Downstream raw materials:

3-(4-methylphenyl)-4(3H)-quinazolinone

3-(4-methylphenyl)benzo-1,2,3-triazin-4(3H)-one

2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-N-p-tolyl-benzamide

2-{[1-(3,4-Dimethoxy-phenyl)-meth-(E)-ylidene]-amino}-N-p-tolyl-benzamide