1,8,15-Triazacyclohenicosane-2,9,16-trione

Base Information

Chemical Name:1,8,15-Triazacyclohenicosane-2,9,16-trione
CAS No.:56403-08-8
Molecular Formula:C18H33N3O3
Molecular Weight:339.478
Hs Code.:
DSSTox Substance ID:DTXSID801031783
Nikkaji Number:J450.664B

Synonyms:56403-08-8;1,8,15-triazacyclohenicosane-2,9,16-trione;1,8,15-Triazacycloheneicosane-2,9,16-trione;Cyclic Trimer of Caprolactam;DTXSID801031783;AS-79333;1,8,15-Triazacyclodocosane-2,9,16-trione

Suppliers and Price of 1,8,15-Triazacyclohenicosane-2,9,16-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,8,15-Triazacyclohenicosane-2,9,16-trione

Chemical Property:

PSA：87.30000
LogP:3.01620
XLogP3:1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:339.25219192
Heavy Atom Count:24
Complexity:329

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=O)NCCCCCC(=O)NCCCCCC(=O)NCC1

Technology Process of 1,8,15-Triazacyclohenicosane-2,9,16-trione

There total 7 articles about 1,8,15-Triazacyclohenicosane-2,9,16-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 56403-08-8
1,8,15-triaza-cycloheneicosane-2,9,16-trione

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

2: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

3: DMF; triethylamine; chlorocarbonic acid isobutyl ester / Reagens 4: THF; anschliessend Behandeln mit Thiophenol in DMF

4: HBr; acetic acid / anschliessend Erhitzen mit wenig Triaethylamin in DMF

With tetrahydrofuran; hydrogen bromide; acetic acid; triethylamine; N,N-dimethyl-formamide; isobutyl chloroformate;

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 56403-08-8
1,8,15-triaza-cycloheneicosane-2,9,16-trione

Guidance literature:: Multi-step reaction with 5 steps

1: chlorocarbonic acid benzyl ester; aqueous NaOH

2: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

3: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

4: DMF; triethylamine; chlorocarbonic acid isobutyl ester / Reagens 4: THF; anschliessend Behandeln mit Thiophenol in DMF

5: HBr; acetic acid / anschliessend Erhitzen mit wenig Triaethylamin in DMF

With tetrahydrofuran; sodium hydroxide; hydrogen bromide; acetic acid; benzyl chloroformate; triethylamine; N,N-dimethyl-formamide; isobutyl chloroformate;

Reference yield:

: 124135-77-9
6-[6-(6-benzyloxycarbonylamino-hexanoylamino)-hexanoylamino]-hexanoic acid hydrazide

: 56403-08-8
1,8,15-triaza-cycloheneicosane-2,9,16-trione

Guidance literature:: With hydrogen bromide; acetic acid; anschliessend Behandeln des Reaktionsprodukts mit wss. HCl und NaNO₂ und Behandeln des erhaltenen Azids mit wss. NaHCO₃;