6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl-

Base Information

Chemical Name:6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl-
CAS No.:59774-28-6
Molecular Formula:C19H19N3O2
Molecular Weight:321.3731
Hs Code.:
DSSTox Substance ID:DTXSID10208510
Nikkaji Number:J240.020K
Wikidata:Q83082627

Synonyms:BRN 0840573;6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl-;59774-28-6;Dimethoxy-1,4-ethyl-5-methyl-6-pyridazino(4,5-b)carbazole;5-Ethyl-1,4-dimethoxy-6-methyl-6H-pyridazino(4,5-b)carbazole;DTXSID10208510;LS-129693;1,4-Dimethoxy-5-ethyl-6-methyl-6H-pyridazino[4,5-b]carbazole

Suppliers and Price of 6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl-

Chemical Property:

Vapor Pressure:4.19E-11mmHg at 25°C
Boiling Point:524.7°Cat760mmHg
Flash Point:271.1°C
Density:1.26g/cm³
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:321.147726857
Heavy Atom Count:24
Complexity:448

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=C2C(=CC3=C1C(=NN=C3OC)OC)C4=CC=CC=C4N2C

Technology Process of 6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl-

There total 5 articles about 6H-Pyridazino(4,5-b)carbazole, 5-ethyl-1,4-dimethoxy-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 124-41-4
sodium methylate

: 59774-23-1
dichloro-1,4 ethyl-5 methyl-6 pyridazino<4,5-b>carbazole

: 59774-28-6
dimethoxy-1,4 ethyl-5 methyl-6 pyridazino<4,5-b>carbazole

Guidance literature:: In methanol; at 150 ℃; for 5h;
DOI:10.1248/cpb.37.2679

Reference yield:

: 59774-11-7
d'ethyl-1 methyl-9 carbazole dicarboxylate de methyle-2,3

: 59774-28-6
dimethoxy-1,4 ethyl-5 methyl-6 pyridazino<4,5-b>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: h2NNH₂*H₂O / 2 h / Heating

2: acetic acid / 0.5 h / Heating

3: 53 percent / POCl₃, pyridine / 14 h / 165 °C

4: 74 percent / methanol / 5 h / 150 °C

With pyridine; hydrazine hydrate; trichlorophosphate; In methanol; acetic acid;
DOI:10.1248/cpb.37.2679

Reference yield:

: 59774-18-4
dioxo-1,4 ethyl-5 methyl-6 tetrahydro-1,2,3,4 pyridazino<4,5-b>carbazole

: 59774-28-6
dimethoxy-1,4 ethyl-5 methyl-6 pyridazino<4,5-b>carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / POCl₃, pyridine / 14 h / 165 °C

2: 74 percent / methanol / 5 h / 150 °C

With pyridine; trichlorophosphate; In methanol;
DOI:10.1248/cpb.37.2679