oxo(diphenyl)germane

Base Information

• Chemical Name: oxo(diphenyl)germane
• CAS No.: 3430-85-1
• Molecular Formula: C12H10GeO
• Molecular Weight: 242.801
• Mol file: 3430-85-1.mol

Synonyms:

Chemical Property of oxo(diphenyl)germane

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of oxo(diphenyl)germane

There total 5 articles about oxo(diphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

dichlorodiphenylgermane (1613-66-7) → diphenylgermanium oxide (3430-85-1)

Guidance literature:

With sodium hydroxide; In ethanol; dichloromethane; water; at 20 ℃; for 72h;

DOI:10.1021/acs.organomet.5b00768

Reference yield: 17.0%

diphenylgermylene (68816-03-5) → benzylidene phenylamine (538-51-2) + diphenylgermanium oxide (3430-85-1)

Guidance literature:

With phenyldiazomethane; Nitrosobenzene; copper; In pentane; PhNO added slowly to mixture of Ph2Ge and PhCHN2 in presence of copper at 40°C;

DOI:10.1021/ja00536a059

Reference yield: 7.0%

diphenylgermylene (68816-03-5) → ethyl 3-phenyl-2-propenoate (103-36-6) + diphenylgermanium oxide (3430-85-1)

Guidance literature:

With diazoacetic acid ethyl ester; benzaldehyde;

DOI:10.1021/ja00536a059

upstream raw materials:

diphenylgermylene

dichlorodiphenylgermane