3-Methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

Base Information

Chemical Name:3-Methyl-1-(3-methylfuran-2-yl)but-2-en-1-one
CAS No.:6138-88-1
Molecular Formula:C10H12O2
Molecular Weight:164.2
Hs Code.:2932190090
DSSTox Substance ID:DTXSID20340399
Nikkaji Number:J13.642E
Wikidata:Q82110016
Mol file:6138-88-1.mol

Synonyms:Naginata ketone;6138-88-1;3-methyl-1-(3-methylfuran-2-yl)but-2-en-1-one;Elsholtzione, .alpha.-dehydro;Naginataketone;Dehydroelsholtzia ketone;DTXSID20340399;AKOS040762986;3-methyl-2-(3-methylbut-2-enoyl)furan;3-Methyl-1-(3-methyl-2-furyl)-2-buten-1-one #

Suppliers and Price of 3-Methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Naginataketone 95+%
5mg
$ 634.00

Total 7 raw suppliers

Chemical Property of 3-Methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

Chemical Property:

Melting Point:145-146℃
Refractive Index:1.5208 (589.3 nm 30℃)
Boiling Point:112-116℃ (20 Torr)
PSA：30.21000
Density:1.0005 g/cm3 (30℃)
LogP:2.73690
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:164.083729621
Heavy Atom Count:12
Complexity:202

Purity/Quality:

98%Min ^*data from raw suppliers

Naginataketone 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(OC=C1)C(=O)C=C(C)C

Technology Process of 3-Methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

There total 9 articles about 3-Methyl-1-(3-methylfuran-2-yl)but-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 22601-06-5
3-methylfuran-2-carbonyl chloride

: 71478-44-9
2-methyl-1-propenylmanganese chloride

: 6138-88-1
3-methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

Guidance literature:: With copper(l) chloride; In tetrahydrofuran; at -10 ℃; for 0.333333h;
DOI:10.1016/S0040-4039(00)79145-3

Reference yield: 61.0%

: 22601-06-5
3-methylfuran-2-carbonyl chloride

: 62485-91-0
iodo-(2-methyl-propenyl)-manganese

: 6138-88-1
3-methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

Guidance literature:: DOI:10.1016/S0040-4039(00)79145-3

Reference yield: 60.0%

: 22601-06-5
3-methylfuran-2-carbonyl chloride

: 18292-39-2
(2-methyl-1-propen-1-yl)trimethylsilane

: 6138-88-1
3-methyl-1-(3-methylfuran-2-yl)but-2-en-1-one

: 78173-38-3
3-Methyl-1-(3-methyl-furan-2-yl)-but-3-en-1-one

: 78173-37-2
3-Chloro-3-methyl-1-(3-methyl-furan-2-yl)-butan-1-one

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -60 - 0 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1016/0040-4039(80)88102-0