Dibutanolamine

Base Information

Chemical Name:Dibutanolamine
CAS No.:21838-75-5
Molecular Formula:C₈H₁₉NO₂
Molecular Weight:161.244
Hs Code.:2922199090
European Community (EC) Number:606-844-1
DSSTox Substance ID:DTXSID60871990
Mol file:21838-75-5.mol

Synonyms:Dibutanolamine;1-(2-hydroxybutylamino)butan-2-ol;21838-75-5;SCHEMBL588144;2-Butanol, 1,1'-iminobis-;1,1'-Azanediyldi(butan-2-ol);DTXSID60871990;1-[(2-hydroxybutyl)amino]butan-2-ol;EN300-7715976

Suppliers and Price of Dibutanolamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Dibutanolamine

Chemical Property:

Melting Point:69 °C
Boiling Point:285.9°Cat760mmHg
PKA:14.53±0.20(Predicted)
Flash Point:111.6°C
PSA：52.49000
Density:0.976g/cm³
LogP:0.50870
XLogP3:0.3
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:161.141578849
Heavy Atom Count:11
Complexity:78.2

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(CNCC(CC)O)O

Technology Process of Dibutanolamine

There total 2 articles about Dibutanolamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183434-54-0
(DL + meso)-N-benzyl-1,1'-iminobis-2-butanol

: 21838-75-5
bis(2-hydroxybutyl)amine

Guidance literature:: With palladium on activated charcoal; In methanol; formic acid; at 20 ℃; for 5h;
DOI:10.1021/tx020095d

Reference yield:

: 106-88-7
ethyloxirane

: 21838-75-5
bis(2-hydroxybutyl)amine

Guidance literature:: With ethanol; ammonia;

Reference yield:

: 21838-75-5
bis(2-hydroxybutyl)amine

: 501364-18-7
5-ethyl-4-methyl-3-hydroxypyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent Chromat_. / tetrahydrofuran / 4 h / 20 °C

2: 83.3 percent Chromat_. / DMSO; oxalyl chloride; triethylamine / CH₂Cl₂ / 3.65 h / -78 - -60 °C

3: 73.0 percent Chromat_. / t-butoxide / tetrahydrofuran / 24 h / 20 °C

With oxalyl dichloride; t-butoxide; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 2: Swern oxidation;
DOI:10.1021/tx020095d