6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl-

Base Information

Chemical Name:6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl-
CAS No.:83948-20-3
Molecular Formula:C₂₄H₃₀N₄O
Molecular Weight:390.528
Hs Code.:2933990090
DSSTox Substance ID:DTXSID60232845
Nikkaji Number:J66.635A
Wikidata:Q83114033
ChEMBL ID:CHEMBL54710
Mol file:83948-20-3.mol

Synonyms:BRN 5634821;83948-20-3;6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl-;1-((3-(Diethylamino)propyl)amino)-5,6-dimethyl-6H-pyrido(4,3-b)carbazol-9-ol;1-[[3-(Diethylamino)propyl]amino]-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-ol;CHEMBL54710;DTXSID60232845;LS-133320

Suppliers and Price of 6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl-

Chemical Property:

Vapor Pressure:1.68E-16mmHg at 25°C
Boiling Point:630.7°Cat760mmHg
Flash Point:335.2°C
PSA：53.32000
Density:1.18g/cm³
LogP:5.11050
XLogP3:5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:390.24196159
Heavy Atom Count:29
Complexity:527

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCCNC1=NC=CC2=C(C3=C(C=C21)C4=C(N3C)C=CC(=C4)O)C

Technology Process of 6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl-

There total 5 articles about 6H-Pyrido(4,3-b)carbazol-9-ol, 1-((3-(diethylamino)propyl)amino)-5,6-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 83947-97-1
1-chloro-9-(benzoyloxy)-5,6-dimethyl-6H-pyrido<4,3-b>carbazole

: 104-78-9
diethylaminopropylamine

: 83948-20-3
1-(3-Diethylamino-propylamino)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-ol

Guidance literature:: at 160 ℃; for 3h;
DOI:10.1021/jm00356a012

Reference yield:

: 72238-06-3
9-hydroxy-5-methyl-6H-pyrido<4,3-b>carbazol-1(2H)-one

: 83948-20-3
1-(3-Diethylamino-propylamino)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 83.8 percent / pyridine / 1 h / Heating

2: 67 percent / phosphorus oxychloride / 3 h / Heating

3: 1.) NaH / 1.) dimethylacetamide, -15 deg C, 30 min, 2.) dimethylacetamide, -15 deg C, 15 h

4: 27 percent / 3 h / 160 °C

With pyridine; sodium hydride; trichlorophosphate;
DOI:10.1021/jm00356a012

Reference yield:

: 83947-95-9
1-chloro-9-(benzoyloxy)-5-methyl-5H-pyrido<4,3-b>carbazole

: 83948-20-3
1-(3-Diethylamino-propylamino)-5,6-dimethyl-6H-pyrido[4,3-b]carbazol-9-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) dimethylacetamide, -15 deg C, 30 min, 2.) dimethylacetamide, -15 deg C, 15 h

2: 27 percent / 3 h / 160 °C

With sodium hydride;
DOI:10.1021/jm00356a012