1-{[(E)-phenylmethylidene]amino}propan-2-ol

Base Information

• Chemical Name: 1-{[(E)-phenylmethylidene]amino}propan-2-ol
• CAS No.: 5456-01-9
• Molecular Formula: C10H13 N O
• Molecular Weight: 163.219

Synonyms:2-Propanol,1-(benzylideneamino)- (8CI); (Benzylidene)(2-hydroxypropyl)amine;1-Benzylideneamino-2-propanol; N-Benzylidene-2-hydroxypropylamine; NSC 7349

Chemical Property of 1-{[(E)-phenylmethylidene]amino}propan-2-ol

Chemical Property:

• Vapor Pressure: 0.00264mmHg at 25°C
• Boiling Point: 274.3°Cat760mmHg
• Flash Point: 160.5°C
• Density: 0.98g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-{[(E)-phenylmethylidene]amino}propan-2-ol

There total 5 articles about 1-{[(E)-phenylmethylidene]amino}propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) + 3-amino-2-propanol (78-96-6,1674-56-2) → N-benzylidene-2-hydroxypropane-1-amine (5456-01-9)

Guidance literature:

DOI:10.1007/BF01153917

Reference yield:

3-amino-2-propanol (78-96-6,1674-56-2) + benzylamine (100-46-9) → N-benzylidene-2-hydroxypropane-1-amine (5456-01-9)

Guidance literature:

With copper(II) on 4-A° molecular sieves; In neat (no solvent); at 120 ℃; for 14h;

DOI:10.1007/s00706-016-1784-9

Reference yield:

2-((trimethylsilyl)oxy)propan-1-amine (17067-54-8) + benzaldehyde (100-52-7) → benzylidene-(2-trimethylsilanyloxy-propyl)-amine + N-benzylidene-2-hydroxypropane-1-amine (5456-01-9)

Guidance literature:

With 4 A molecular sieve; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/b705081j

upstream raw materials:

benzaldehyde

3-amino-2-propanol

2-((trimethylsilyl)oxy)propan-1-amine

benzylamine

Downstream raw materials:

3-benzylaminopropan-2-ol

cis-1-(hydroxypropyl)-3-phenoxy-4-phenylazetidin-2-one

N-{2-[(trimethylsilyl)oxy]propyl}benzimidoyl cyanide

3-hydroxy-1-(2-hydroxypropyl)-4-(4-methylbenzoyl)-5-phenyl-1,5-dihydropyrrol-2-one

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