N-BENZOYL-D-GLUCOSAMINE

Base Information

• Chemical Name: N-BENZOYL-D-GLUCOSAMINE
• CAS No.: 61949-16-4
• Molecular Formula: C13H17NO6
• Molecular Weight: 283.2772
• Hs Code.: 29400090

Synonyms:2-deoxy-2-benzamido-D-glucopyranose;2-Benzoylamino-2-desoxy-D-glucose;2-Benzoylamino-2-desoxy-D-glucopyranose;2-benzamido-2-deoxy-D-glucopyranose;2-Benzamido-2-deoxy-D-glucose;2-benzoylamino-D-2-deoxy-glucose;查看更多英文别名收起

Chemical Property of N-BENZOYL-D-GLUCOSAMINE

Chemical Property:

• Vapor Pressure: 1.75E-17mmHg at 25°C
• Refractive Index: 1.641
• Boiling Point: 644.349 °C at 760 mmHg
• Flash Point: 343.49 °C
• PSA: 119.25000
• Density: 1.48 g/cm³
• LogP: -1.39280
• Storage Temp.: 2-8°C

Purity/Quality:

2-Benzamido-2-deoxy-D-glucopyranose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of N-BENZOYL-D-GLUCOSAMINE

There total 11 articles about N-BENZOYL-D-GLUCOSAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-deoxy-2-amino glucose (90-76-6,90-77-7,530-23-4,579-32-8,579-33-9,643-68-5,2596-19-2,6490-68-2,6490-70-6,6490-72-8,6490-73-9,6490-74-0,14196-84-0,14196-86-2,14257-69-3,58381-21-8) + benzoic acid anhydride (93-97-0) → N-benzoyl-D-glucosamine (6847-14-9,14086-91-0,19949-63-4,61949-16-4)

Guidance literature:

In methanol; at 20 ℃; for 16h;

DOI:10.1016/S0968-0896(02)00213-4

Reference yield: 91.0%

(+)-D-glucosamine hydrochloride (1078691-95-8) + benzoic acid anhydride (93-97-0) → N-benzoyl-D-glucosamine (6847-14-9,14086-91-0,19949-63-4,61949-16-4)

Guidance literature:

(+)-D-glucosamine hydrochloride; With sodium methylate; In methanol; for 0.166667h;

benzoic acid anhydride; In methanol; for 0.5h;

DOI:10.1007/s00706-003-0086-1

Reference yield: 90.0%

(+)-D-glucosamine hydrochloride (1078691-95-8) + benzoic acid (65-85-0,8013-63-6) → N-benzoyl-D-glucosamine (6847-14-9,14086-91-0,19949-63-4,61949-16-4)

Guidance literature:

With 3,3'-(phenylphosphinylidene)bis<2(3H)-benzothiazolone; In sulfolane; for 24h; Ambient temperature;

DOI:10.1246/bcsj.58.3291

upstream raw materials:

p-nitrophenylbenzoate

(+)-D-glucosamine hydrochloride

benzoyl chloride

benzoic acid

Downstream raw materials:

5'.6'-O-Isopropyliden-2-phenyl-α-D-glucofuranol<2'.1':4.5>-Δ²-oxazolin

Benzyl-N-benzoyl-D-glucosaminid

2-Benzamido-2-deoxy-4,6-O-ethylidene-D-glucitol

Methanesulfonic acid (R)-((2R,4S,5R)-5-methanesulfonyloxy-2-methyl-[1,3]dioxan-4-yl)-((S)-2-phenyl-4,5-dihydro-oxazol-4-yl)-methyl ester

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