Phenyl 3,3-diphenylprop-2-enoate

Base Information

Chemical Name:Phenyl 3,3-diphenylprop-2-enoate
CAS No.:5472-00-4
Molecular Formula:C21H16O2
Molecular Weight:300.357
Hs Code.:
NSC Number:28492
DSSTox Substance ID:DTXSID20282861
Nikkaji Number:J1.660.813K

Synonyms:5472-00-4;phenyl 3,3-diphenylprop-2-enoate;NSC28492;DTXSID20282861;NSC-28492

Suppliers and Price of Phenyl 3,3-diphenylprop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Phenyl 3,3-diphenylprop-2-enoate

Chemical Property:

Vapor Pressure:2.55E-08mmHg at 25°C
Boiling Point:450.8°Cat760mmHg
Flash Point:190.8°C
Density:1.144g/cm³
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:300.115029749
Heavy Atom Count:23
Complexity:374

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=CC(=O)OC2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Phenyl 3,3-diphenylprop-2-enoate

There total 8 articles about Phenyl 3,3-diphenylprop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 93501-23-6
2-Bromo-3,3-diphenyl-propionic acid phenyl ester

: 5472-00-4
phenyl 3,3-diphenylpropenoate

Guidance literature:: With 2,4,6-trimethyl-pyridine; Heating;

Reference yield:

: 606-84-8
3,3-diphenylacrylic acid

: 108-95-2,27073-41-2
phenol

: 5472-00-4
phenyl 3,3-diphenylpropenoate

Guidance literature:: With dmap; ethylene dichloride hydrochloride; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201304492

Reference yield:

: 119-61-9
benzophenone

: 5472-00-4
phenyl 3,3-diphenylpropenoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 - 20 °C / Inert atmosphere

2.1: pyridine; thionyl chloride / dichloromethane / 3.17 h / 0 - 20 °C / Inert atmosphere

3.1: potassium hydroxide / tetrahydrofuran; water / 48 h / 90 °C / Inert atmosphere

4.1: dmap; ethylene dichloride hydrochloride / dichloromethane / 12 h / 20 °C / Inert atmosphere

With pyridine; dmap; n-butyllithium; thionyl chloride; ethylene dichloride hydrochloride; potassium hydroxide; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1002/anie.201304492