Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane

Base Information

Chemical Name:Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane
CAS No.:61217-41-2
Molecular Formula:C22H21BiCl2O4
Molecular Weight:629.2861
Hs Code.:
DSSTox Substance ID:DTXSID40586752
NSC Number:370494

Synonyms:61217-41-2;Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane;DTXSID40586752;NSC370494;AKOS024432894;NSC-370494;Bismuth, bis(chloroacetato-O)triphenyl-;TRIPHENYLBISMUTH BIS(2-CHLOROACETATE)

Suppliers and Price of Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:626.04644
Heavy Atom Count:29
Complexity:497

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Bi](C2=CC=CC=C2)(C3=CC=CC=C3)(OC(=O)CCl)OC(=O)CCl

Technology Process of Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane

There total 4 articles about Bis[(chloroacetyl)oxy](triphenyl)-lambda~5~-bismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 47252-14-2
triphenylbismuth carbonate

: 79-11-8
chloroacetic acid

: 61217-41-2
triphenylbismuth bis(monochloroacetate)

Guidance literature:: In acetone; at 56 °C, 30 min;
DOI:10.1021/ja01153a518

Reference yield: 82.0%

: 28899-97-0,7239-60-3
triphenylbismuth(V) diacetate

: 79-11-8
chloroacetic acid

: 61217-41-2
triphenylbismuth bis(monochloroacetate)

Guidance literature:: In dichloromethane; the acid is added to a stirred soln. of the bismuth acetate in CH2Cl2 at room temp., reaction time 30 min; filtd., the solvent is distd., the residue is recrystd. (CH2Cl2/petroleum ether);
DOI:10.1080/00397919408020774