1,2,3-Triiodobenzene

Base Information

Chemical Name:1,2,3-Triiodobenzene
CAS No.:608-29-7
Molecular Formula:C6H3I3
Molecular Weight:455.803
Hs Code.:
DSSTox Substance ID:DTXSID50209642
Nikkaji Number:J134.630J
Wikidata:Q83084006

Synonyms:1,2,3-TRIIODOBENZENE;Benzene, 1,2,3-triiodo-;608-29-7;TRIIODOBENZENE;SCHEMBL38083;DTXSID50209642

Suppliers and Price of 1,2,3-Triiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,2,3-Triiodobenzene

Chemical Property:

Vapor Pressure:8.67E-05mmHg at 25°C
Melting Point:116°C
Refractive Index:1.8070 (estimate)
Boiling Point:350.8°Cat760mmHg
Flash Point:183.3°C
PSA：0.00000
Density:2.928g/cm³
LogP:3.50040
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:455.7369
Heavy Atom Count:9
Complexity:84.3

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)I)I)I

Technology Process of 1,2,3-Triiodobenzene

There total 7 articles about 1,2,3-Triiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2,6-diiodobenzoic acid

: 608-29-7
1,2,3-triiodobenzene

Guidance literature:: With N-iodo-succinimide; In 1,2-dichloro-ethane; for 24h; Photolysis; Reflux;
DOI:10.1071/CH14386

Reference yield: 34.0%

: 108673-30-9
3,4,5-triiodoaniline

: 634-92-4
1,2,3,5-tetraiodobenzene

: 608-29-7
1,2,3-triiodobenzene

Guidance literature:: With isopentyl nitrite; In tetrahydrofuran; Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1021/jo00020a036

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 608-29-7
1,2,3-triiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; iodine; [bis(acetoxy)iodo]benzene / N,N-dimethyl-formamide / 24 h / 100 °C / Sealed tube

2: N-iodo-succinimide / 1,2-dichloro-ethane / 24 h / Photolysis; Reflux

With N-iodo-succinimide; [bis(acetoxy)iodo]benzene; iodine; palladium diacetate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1071/CH14386