Technology Process of 1,2,3-Triiodobenzene
There total 7 articles about 1,2,3-Triiodobenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide;
In
1,2-dichloro-ethane;
for 24h;
Photolysis;
Reflux;
DOI:10.1071/CH14386
- Guidance literature:
-
With
isopentyl nitrite;
In
tetrahydrofuran;
Yields of byproduct given. Title compound not separated from byproducts;
Heating;
DOI:10.1021/jo00020a036
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium diacetate; iodine; [bis(acetoxy)iodo]benzene / N,N-dimethyl-formamide / 24 h / 100 °C / Sealed tube
2: N-iodo-succinimide / 1,2-dichloro-ethane / 24 h / Photolysis; Reflux
With
N-iodo-succinimide; [bis(acetoxy)iodo]benzene; iodine; palladium diacetate;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1071/CH14386
