Technology Process of 2-methyl-1-pentofuranosyl-1,2-dihydropyridine-3,4-diol
There total 4 articles about 2-methyl-1-pentofuranosyl-1,2-dihydropyridine-3,4-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium;
In
methanol;
under 760 Torr;
DOI:10.1021/jm00368a010
- Guidance literature:
-
Multi-step reaction with 4 steps
1: K2CO3 / acetone / 72 h / Ambient temperature
2: ethanol, NH4OH / Heating
3: 1.) hexamethyldisilazane, ammonium sulfate, 2.) trimethylsilyl trifluoromethanesulfonate / 1.) reflux, 2 h, 2.) CH3CN, RT, 24 h
4: 0.98 g / H2 / Pd black / methanol / 760 Torr
With
ammonium hydroxide; ammonium sulfate; ethanol; trimethylsilyl trifluoromethanesulfonate; hydrogen; potassium carbonate; 1,1,1,3,3,3-hexamethyl-disilazane;
palladium;
In
methanol; acetone;
DOI:10.1021/jm00368a010
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) hexamethyldisilazane, ammonium sulfate, 2.) trimethylsilyl trifluoromethanesulfonate / 1.) reflux, 2 h, 2.) CH3CN, RT, 24 h
2: 0.98 g / H2 / Pd black / methanol / 760 Torr
With
ammonium sulfate; trimethylsilyl trifluoromethanesulfonate; hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane;
palladium;
In
methanol;
DOI:10.1021/jm00368a010
