Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI)

Base Information

Chemical Name:Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI)
CAS No.:100752-88-3
Molecular Formula:C₈H₁₃NO
Molecular Weight:139.197
Hs Code.:
Mol file:100752-88-3.mol

Synonyms:Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI);isoarecolone

Suppliers and Price of Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(1,2,3,6-TETRAHYDRO-1-METHYL-4-PYRIDINYL)-ETHANONE 95.00%
5MG
$ 497.39

Total 5 raw suppliers

Chemical Property of Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI)

Chemical Property:

Vapor Pressure:0.0844mmHg at 25°C
Boiling Point:225.9°Cat760mmHg
PKA:8.09±0.40(Predicted)
Flash Point:80.8°C
PSA：20.31000
Density:0.993g/cm³
LogP:0.77520

Purity/Quality:

99% ^*data from raw suppliers

1-(1,2,3,6-TETRAHYDRO-1-METHYL-4-PYRIDINYL)-ETHANONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI)

There total 7 articles about Ethanone, 1-(1,2,3,6-tetrahydro-1-methyl-4-pyridinyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 112654-70-3
1-methyl-4-(2-hydroxyethyl)-1,2,3,6-tetrahydropyridine

: 100752-88-3
1-(1,2,3,6-Tetrahydro-1-methyl-4-pyridinyl)-ethanone

Guidance literature:: With chromium(VI) oxide; In acetic acid; for 1.25h;
DOI:10.1021/jm00398a010

Reference yield:

: 7630-04-8
1-methyl-4-acetylpyridinium iodide

: 100752-88-3
1-(1,2,3,6-Tetrahydro-1-methyl-4-pyridinyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaBH₄ / methanol / 0.5 h / 21 °C

2: 18 percent / CrO₃ / acetic acid / 1.25 h

With chromium(VI) oxide; sodium tetrahydroborate; In methanol; acetic acid;
DOI:10.1021/jm00398a010

Reference yield:

: 60553-34-6
1-methyl-4-(2-methyl-1,3-dioxolan-2-yl)pyridinium iodide

: 100752-88-3
1-(1,2,3,6-Tetrahydro-1-methyl-4-pyridinyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaBH₄ / ethanol / 1 h / 0 - 5 °C

2: 1percent aq. H₂SO₄ / 2 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; In ethanol;
DOI:10.1002/jhet.5570340637