6,7-diethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride

Base Information

• Chemical Name: 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride
• CAS No.: 63937-90-6
• Molecular Formula: C₁₄H₂₁NO₂*ClH
• Molecular Weight: 271.787
• Mol file: 63937-90-6.mol

Synonyms:Isoquinoline,6,7-diethoxy-1,2,3,4-tetrahydro-2-methyl-, hydrochloride (9CI)

Chemical Property of 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride

Chemical Property:

• Vapor Pressure: 0.000151mmHg at 25°C
• Boiling Point: 331.9°Cat760mmHg
• Flash Point: 111.6°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride

There total 3 articles about 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3,4-diethoxyphenyl)ethylamine (61381-04-2) → 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride (63937-90-6)

Guidance literature:

Multi-step reaction with 2 steps

2: water / und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure

With water;

DOI:10.1021/ja01283a038

Reference yield:

3-(3,4-diethoxy-phenyl)-propionic acid amide (857792-10-0) → 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride (63937-90-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hypochlorite

3: water / und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure

With sodium hypochlorite; water;

DOI:10.1021/ja01283a038

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + (3,4-diethoxy-phenethyl)-methyl-amine (21581-36-2) → 6,7-diethoxy-2-methyl-1,2,3,4-tetrahydro-isoquinoline; hydrochloride (63937-90-6)

Guidance literature:

With water; und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure;

DOI:10.1021/ja01283a038

upstream raw materials:

formaldehyd

(3,4-diethoxy-phenethyl)-methyl-amine

2-(3,4-diethoxyphenyl)ethylamine

3-(3,4-diethoxy-phenyl)-propionic acid amide