Technology Process of Phosphorous chloridediiodide (9CI)
There total 1 articles about Phosphorous chloridediiodide (9CI) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
carbon disulfide;
under N2, dropwise addn. of a Br2/CS2 soln. to a vigorously stirred soln. of P4/CS2 reaction of P4 with ICl (molar ratio (1.75:1.5), further Products: ClIP2ClI, ClIP2I2, P2I4, P7I3; not isolated, identified by 31P-NMR spectroscopy;
DOI:10.1016/S0277-5387(00)83446-4