3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one

Base Information

Chemical Name:3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one
CAS No.:105889-14-3
Molecular Formula:C₁₂H₁₃ClN₂O₂
Molecular Weight:252.7
Hs Code.:
DSSTox Substance ID:DTXSID30909794

Synonyms:BRN 5556412;105889-14-3;2H-1,3,4-Oxadiazin-2-one, 3,6-dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-;3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one;DTXSID30909794;LS-98982;6-(4-Chlorophenyl)-3,5,6-trimethyl-3,6-dihydro-2H-1,3,4-oxadiazin-2-one

Suppliers and Price of 3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one

Chemical Property:

Vapor Pressure:0.000254mmHg at 25°C
Boiling Point:323.9°Cat760mmHg
Flash Point:149.7°C
Density:1.26g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:252.0665554
Heavy Atom Count:17
Complexity:350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN(C(=O)OC1(C)C2=CC=C(C=C2)Cl)C

Technology Process of 3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one

There total 3 articles about 3,6-Dihydro-6-(p-chlorophenyl)-3,5,6-trimethyl-2H-1,3,4-oxadiazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N'-[2-(4-Chloro-phenyl)-2-hydroxy-1-methyl-prop-(E)-ylidene]-hydrazinecarboxylic acid ethyl ester

: 105889-14-3
6-(4-Chloro-phenyl)-3,5,6-trimethyl-3,6-dihydro-[1,3,4]oxadiazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / 2-methyl-propan-2-ol; benzene / 40 h / Heating

2: 1) NaOEt / 1) EtOH, 12 h, RT, 2) EtOH, 48 h, 30 deg C

With potassium tert-butylate; sodium ethanolate; In tert-butyl alcohol; benzene;

Reference yield:

: N'-[2-(4-Chloro-phenyl)-2-hydroxy-1-methyl-prop-(E)-ylidene]-hydrazinecarboxylic acid methyl ester

: 105889-14-3
6-(4-Chloro-phenyl)-3,5,6-trimethyl-3,6-dihydro-[1,3,4]oxadiazin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / 2-methyl-propan-2-ol; benzene / 40 h / Heating

2: 1) NaOEt / 1) EtOH, 12 h, RT, 2) EtOH, 48 h, 30 deg C

With potassium tert-butylate; sodium ethanolate; In tert-butyl alcohol; benzene;