2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate

Base Information

Chemical Name:2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate
CAS No.:64228-80-4
Molecular Formula:2CH₃O₃S*C₅₃H₇₂N₂O₁₂
Molecular Weight:1119.36
Hs Code.:
European Community (EC) Number:264-742-9

2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate

Synonyms:EINECS 264-742-9;64228-80-4;2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate;2,2'-[1,5-pentanediylbis[oxy(3-oxo-3,1-propanediyl)]]bis[1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium] dimethanesulphonate;C53H72N2O12.2CH3O3S;C53-H72-N2-O12.2C-H3-O3-S;2,2'-((Pentane-1,5-diylbis(oxy))bis(3-oxopropane-3,1-diyl))bis(1-(3,4-dimethoxybenzyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinolin-2-ium) methanesulfonate

Suppliers and Price of 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:18
Rotatable Bond Count:26
Exact Mass:1118.46910599
Heavy Atom Count:77
Complexity:1470

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1(CCC2=CC(=C(C=C2C1CC3=CC(=C(C=C3)OC)OC)OC)OC)CCC(=O)OCCCCCOC(=O)CC[N+]4(CCC5=CC(=C(C=C5C4CC6=CC(=C(C=C6)OC)OC)OC)OC)C.CS(=O)(=O)[O-].CS(=O)(=O)[O-]

Technology Process of 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate

There total 6 articles about 2,2'-(1,5-Pentanediylbis(oxy(3-oxo-3,1-propanediyl)))bis(1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinolinium) dimethanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 66-27-3
Methyl methanesulfonate

: 64228-78-0,64493-10-3,83285-74-9,96687-52-4,96687-53-5,110817-20-4
pentamethylene bis(1-(3,4-dimethoxybenzyl)-3,4-dihydro-6,7-dimethoxy-1H-isoquinoline-2-propionate) dioxalate

: 64228-80-4,64228-99-5,64264-70-6,64541-71-5,96946-40-6,141196-63-6
C₅₃H₇₂N₂O₁₂⁽²⁺⁾*2CH₃O₃S^(1-)

Guidance literature:: In acetonitrile; for 48h; Ambient temperature;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 64228-80-4,64228-99-5,64264-70-6,64541-71-5,96946-40-6,141196-63-6
C₅₃H₇₂N₂O₁₂⁽²⁺⁾*2CH₃O₃S^(1-)

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / 2 h / 190 - 210 °C

2: phosphoryl chloride / toluene / 3 h / Heating

3: 71 percent / sodium borohydride / 19 h / Ambient temperature

4: 51 percent / benzene / 48 h / Heating

5: 80 percent / acetonitrile / 48 h / Ambient temperature

With sodium tetrahydroborate; trichlorophosphate; In toluene; acetonitrile; benzene;

Reference yield:

: 139-76-4
N-(3,4-dimethoxyphenethyl)-2-(3,4-dimethoxyphenyl)acetamide

: 64228-80-4,64228-99-5,64264-70-6,64541-71-5,96946-40-6,141196-63-6
C₅₃H₇₂N₂O₁₂⁽²⁺⁾*2CH₃O₃S^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1: phosphoryl chloride / toluene / 3 h / Heating

2: 71 percent / sodium borohydride / 19 h / Ambient temperature

3: 51 percent / benzene / 48 h / Heating

4: 80 percent / acetonitrile / 48 h / Ambient temperature

With sodium tetrahydroborate; trichlorophosphate; In toluene; acetonitrile; benzene;