N-1-Naphthylsalicylamide

Base Information

• Chemical Name: N-1-Naphthylsalicylamide
• CAS No.: 5343-69-1
• Molecular Formula: C17H13NO2
• Molecular Weight: 263.2906
• NSC Number: 486
• DSSTox Substance ID: DTXSID50968101
• Wikidata: Q82950797

Synonyms:5343-69-1;N-1-NAPHTHYLSALICYLAMIDE;NSC486;Bio6B2;Oprea1_567914;SCHEMBL331600;CCG-713;DTXSID50968101;NSC-486;AKOS000212916;Z56871873;2-Hydroxy-N-(naphthalen-1-yl)benzene-1-carboximidic acid

Chemical Property of N-1-Naphthylsalicylamide

Chemical Property:

• Vapor Pressure: 1.07E-06mmHg at 25°C
• Boiling Point: 391.8°Cat760mmHg
• Flash Point: 190.7°C
• Density: 1.31g/cm³
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 263.094628657
• Heavy Atom Count: 20
• Complexity: 344

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2NC(=O)C3=CC=CC=C3O

Technology Process of N-1-Naphthylsalicylamide

There total 4 articles about N-1-Naphthylsalicylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-amino-naphthalene (134-32-7) + salicylic acid (69-72-7,25496-36-0,8052-31-1) → salicyl naphth-1-ylamine (5343-69-1)

Guidance literature:

With phosphorus trichloride; In 5,5-dimethyl-1,3-cyclohexadiene; for 0.75h; Microwave irradiation;

DOI:10.1080/00397911.2010.481745

Reference yield: 84.0%

1-Naphthyl isocyanate (86-84-0) + phenol (108-95-2,27073-41-2) → salicyl naphth-1-ylamine (5343-69-1)

Guidance literature:

boron trichloride; In dichloromethane; Heating;

DOI:10.1016/S0040-4020(01)87495-0

Reference yield:

1-amino-naphthalene (134-32-7) + salicyloyl chloride (1441-87-8) → salicyl naphth-1-ylamine (5343-69-1)

Guidance literature:

With benzene;

DOI:10.1007/BF01532301

upstream raw materials:

1-amino-naphthalene

salicylic acid

salicyloyl chloride

1-Naphthyl isocyanate

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