2-AMINO-5-FLUORO-3-NITROBENZOTRIFLUORIDE

Base Information

• Chemical Name: 2-AMINO-5-FLUORO-3-NITROBENZOTRIFLUORIDE
• CAS No.: 344-29-6
• Molecular Formula: C7H4F4N2O2
• Molecular Weight: 224.115
• Hs Code.: 2921420090
• Mol file: 344-29-6.mol

Synonyms:2-Amino-5-fluoro-3-nitrobenzotrifluoride;4-Fluor-2-nitro-6-trifluormethyl-anilin;4-fluoro-2-nitro-6-trifluoromethyl-aniline;

Chemical Property of 2-AMINO-5-FLUORO-3-NITROBENZOTRIFLUORIDE

Chemical Property:

• Vapor Pressure: 0.0114mmHg at 25°C
• Boiling Point: 261.6°Cat760mmHg
• PKA: -2.82±0.25(Predicted)
• Flash Point: 112°C
• PSA: 71.84000
• Density: 1.586g/cm³
• LogP: 3.43930
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-5-fluoro-3-nitrobenzotrifluoride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Amino-5-fluoro-3-nitrobenzotrifluoride is a useful research intermediate, a substituted benzotrifluorides.

Technology Process of 2-AMINO-5-FLUORO-3-NITROBENZOTRIFLUORIDE

There total 3 articles about 2-AMINO-5-FLUORO-3-NITROBENZOTRIFLUORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

acetic acid-(4-fluoro-2-nitro-6-trifluoromethyl-anilide) (389-75-3) → 4-fluoro-2-nitro-6-trifluoromethyl-aniline (344-29-6)

Guidance literature:

In hydrogenchloride;

Reference yield:

N-(4-fluoro-2-(trifluoromethyl)phenyl)acetamide (393-23-7) → 4-fluoro-2-nitro-6-trifluoromethyl-aniline (344-29-6)

Guidance literature:

Multi-step reaction with 2 steps

1: concd. H₂SO₄, concd. HNO₃ / 0 - 20 °C

2: concd. HCl / Heating

With hydrogenchloride; sulfuric acid; nitric acid;

DOI:10.1021/jm00022a003

Reference yield:

4-fluoro-2-(trifluoromethyl)aniline (393-39-5) → 4-fluoro-2-nitro-6-trifluoromethyl-aniline (344-29-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 12 h / 25 °C

2: concd. H₂SO₄, concd. HNO₃ / 0 - 20 °C

3: concd. HCl / Heating

With hydrogenchloride; sulfuric acid; nitric acid;

DOI:10.1021/jm00022a003

upstream raw materials:

acetic acid-(4-fluoro-2-nitro-6-trifluoromethyl-anilide)

4-fluoro-2-(trifluoromethyl)aniline

N-(4-fluoro-2-(trifluoromethyl)phenyl)acetamide

Downstream raw materials:

2,3-diamino-5-fluorobenzotrifluoride

quinoxaline-2,3-dione

7-fluoro-2,3-diphenyl-5-trifluoromethyl-quinoxaline

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