2-(9-Oxoxanthen-2-yl)propionic Acid

Base Information

Chemical Name:2-(9-Oxoxanthen-2-yl)propionic Acid
CAS No.:30087-33-3
Molecular Formula:C16H12 O4
Molecular Weight:268.269
Hs Code.:
European Community (EC) Number:805-889-6
DSSTox Substance ID:DTXSID80952497
Nikkaji Number:J395.397A
Mol file:30087-33-3.mol

Synonyms:9-oxoxanthen-2-yl-alpha-propionic acid;Y 5554;Y-5554

Suppliers and Price of 2-(9-Oxoxanthen-2-yl)propionic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
2-(9-Oxoxanthen-2-yl)propionic Acid >98.0%(GC)(T)
1g
$ 325.00

Crysdot
2-(9-Oxo-9H-xanthen-2-yl)propanoicacid 97%
5g
$ 630.00

Chem-Impex
2-(9-Oxoxanthen-2-yl)propionicacid,≥98%(GC) ≥98%(GC)
1G
$ 372.09

AK Scientific
2-(9-Oxoxanthen-2-yl)propionic Acid
1g
$ 486.00

Total 8 raw suppliers

Chemical Property of 2-(9-Oxoxanthen-2-yl)propionic Acid

Chemical Property:

Vapor Pressure:3.16E-10mmHg at 25°C
Melting Point:164.0 to 174.0 °C
Boiling Point:485.2°Cat760mmHg
Flash Point:185.9°C
PSA：67.51000
Density:1.352g/cm³
LogP:3.13430
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:268.07355886
Heavy Atom Count:20
Complexity:405

Purity/Quality:

97% ^*data from raw suppliers

2-(9-Oxoxanthen-2-yl)propionic Acid >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=CC2=C(C=C1)OC3=CC=CC=C3C2=O)C(=O)O

Technology Process of 2-(9-Oxoxanthen-2-yl)propionic Acid

There total 4 articles about 2-(9-Oxoxanthen-2-yl)propionic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₄O₅

: 30087-33-3
2-(9-oxoxanthene-2-yl)propionic acid

Guidance literature:: With sulfuric acid; at 85 ℃; for 2h;
DOI:10.1016/j.bmcl.2014.11.084

Reference yield:

: 78096-25-0
2-xanthoneacetic acid methyl ester

: 74-88-4
methyl iodide

: 30087-33-3
2-(9-oxoxanthene-2-yl)propionic acid

Guidance literature:: 2-xanthoneacetic acid methyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at -78 - 20 ℃; Further stages; Inert atmosphere;

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 30087-33-3
2-(9-oxoxanthene-2-yl)propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / 1,4-dioxane / 0.17 h / 20 °C / Inert atmosphere

1.2: Inert atmosphere; Reflux

2.1: sulfuric acid / 2 h / 85 °C

With sulfuric acid; caesium carbonate; In 1,4-dioxane; 1.1: |Ullmann Condensation / 2.1: |Friedel-Crafts Acylation;
DOI:10.1016/j.bmcl.2014.11.084