Technology Process of 6-Heneicosyn-11-ol
There total 7 articles about 6-Heneicosyn-11-ol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1-iodo-4-decyne;
With
iodine; magnesium;
In
diethyl ether;
Heating;
undecylaldehyde;
In
diethyl ether;
at 0 ℃;
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
DOI:10.1021/jo00899a016
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium, liquid ammonia, FeCl3 / 0.17 h
2: aq. 10percent H2SO4 / methanol; H2O / 1 h / Ambient temperature
3: 90 percent / hydrogen peroxide, potassium hydroxide / methanol; H2O / 1 h / 15 °C
4: 7.8 g / tosyl hydrazine / acetic acid; CH2Cl2 / 8 h / Ambient temperature
5: 2.2 g / tetrahydrofuran / 3 h / Ambient temperature
With
potassium hydroxide; sulfuric acid; ammonia; dihydrogen peroxide; potassium; iron(III) chloride; toluene-4-sulfonic acid hydrazide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetic acid;
DOI:10.1039/P19830000007