O-cyclohexylhydroxylamine

Base Information

Chemical Name:O-cyclohexylhydroxylamine
CAS No.:4759-21-1
Molecular Formula:C₆H₁₃NO
Molecular Weight:115.175
Hs Code.:
European Community (EC) Number:688-893-9
DSSTox Substance ID:DTXSID10445286
Nikkaji Number:J2.343.199H
Wikidata:Q82263651
Mol file:4759-21-1.mol

Synonyms:O-cyclohexylhydroxylamine;4759-21-1;Cyclohexyloxyamin;(aminooxy)cyclohexane;SCHEMBL441840;DTXSID10445286;KYKNGOPXRHUCHC-UHFFFAOYSA-N;MFCD12031675;AKOS006316942;CS-0210389;EN300-141060

Suppliers and Price of O-cyclohexylhydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of O-cyclohexylhydroxylamine

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:115.099714038
Heavy Atom Count:8
Complexity:59.5

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)ON

Technology Process of O-cyclohexylhydroxylamine

There total 6 articles about O-cyclohexylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 169956-61-0
2-(cyclohexyloxy)-1H-isoindole-1,3(2H)-dione

: 4759-21-1
O-cyclohexyl-hydroxylamine

Guidance literature:: With hydrazine hydrate; In methanol; dichloromethane; at 20 ℃; for 8h;
DOI:10.1021/jm4009949

Reference yield:

: 108-93-0
cyclohexanol

: 4759-21-1
O-cyclohexyl-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 5 h / 0 - 20 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 1.5 h / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1002/anie.202110019

Reference yield:

: 108-93-0
cyclohexanol

: 4759-21-1
O-cyclohexyl-hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: DEAD, PPh₃ / tetrahydrofuran

2: NH₂NH₂*H₂O / ethanol / Heating

With hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol;
DOI:10.1016/0223-5234(94)90027-2