Technology Process of 4-ethyl-5-hydroxy-2,2-dimethylcyclopent-4-ene-1,3-dione
There total 6 articles about 4-ethyl-5-hydroxy-2,2-dimethylcyclopent-4-ene-1,3-dione which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / hydrogen, sodium carbonate / 5 percent Pd/C / methanol; H2O / 2250.2 - 3000.2 Torr / Ambient temperature
2: chlorine / CCl4
3: chlorine / CCl4; dimethylformamide / 0.42 h / Heating
4: conc. hydrochloric acid, potassium iodide, sodium metabisulfite / CH2Cl2; methanol / 20 - 35 °C
5: 2 N sodium hydroxide / H2O; methanol / Ambient temperature
With
hydrogenchloride; sodium hydroxide; sodium disulfite; hydrogen; chlorine; sodium carbonate; potassium iodide;
palladium on activated charcoal;
In
methanol; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: chlorine / CCl4
2: chlorine / CCl4; dimethylformamide / 0.42 h / Heating
3: conc. hydrochloric acid, potassium iodide, sodium metabisulfite / CH2Cl2; methanol / 20 - 35 °C
4: 2 N sodium hydroxide / H2O; methanol / Ambient temperature
With
hydrogenchloride; sodium hydroxide; sodium disulfite; chlorine; potassium iodide;
In
methanol; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
With
sodium hydroxide;
In
methanol; water;
Ambient temperature;