BenzaMide, N,N-diethyl-3-nitro-

Base Information

• Chemical Name: BenzaMide, N,N-diethyl-3-nitro-
• CAS No.: 2433-21-8
• Molecular Formula: C11H14 N2 O3
• Molecular Weight: 222.244
• Hs Code.: 2924299090
• Mol file: 2433-21-8.mol

Synonyms:Benzamide,N,N-diethyl-m-nitro- (7CI); N,N-Diethyl-3-nitrobenzamide;N,N-Diethyl-m-nitrobenzamide; NSC 406568

Chemical Property of BenzaMide, N,N-diethyl-3-nitro-

Chemical Property:

• Vapor Pressure: 1.14E-05mmHg at 25°C
• Boiling Point: 370°Cat760mmHg
• Flash Point: 177.6°C
• PSA: 66.13000
• Density: 1.172g/cm³
• LogP: 2.60000

Purity/Quality:

97% ^*data from raw suppliers

N,N-Diethyl-3-nitrobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BenzaMide, N,N-diethyl-3-nitro-

There total 6 articles about BenzaMide, N,N-diethyl-3-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

m-iodonitrobenzene (645-00-1) + carbon monoxide (201230-82-2) + triethylamine (121-44-8) → N,N-diethyl-3-nitrobenzamide (2433-21-8)

Guidance literature:

With palladium 10% on activated carbon; oxygen; In acetonitrile; at 100 ℃; for 8h; under 4560.31 Torr; Autoclave; Green chemistry;

DOI:10.1021/acs.joc.5b02385

Reference yield: 93.0%

disulfiram (97-77-8) + 3-nitrobenzoic acid (121-92-6) → N,N-diethyl-3-nitrobenzamide (2433-21-8)

Guidance literature:

With di-tert-butyl peroxide; copper(I) bromide; In ethyl acetate; at 120 ℃;

DOI:10.1080/00397911.2017.1330960

Reference yield: 45.0%

triethylamine (121-44-8) + 3-nitrobenzoic acid (121-92-6) → N,N-diethyl-3-nitrobenzamide (2433-21-8)

Guidance literature:

With iodine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tetlet.2015.12.009

upstream raw materials:

diethylamine

m-nitrobenzoic acid chloride

N,N-diethylbenzamide

3-nitrobenzoic acid

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