Technology Process of Diaporthin
There total 10 articles about Diaporthin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 80.6 percent / sodium ethoxyde / ethanol / Heating
2: 97.6 percent / potassium hydroxide, 18-crown-6 / H2O; dioxane
3: 89.1 percent / trifluoroacetic anhydride
4: 1.) mercuric acetate; 2.) sodium borohydride / 1.) water, THF, r.t.
6: 1.) ozon; 2.) dimethyl sulfide / 1.) ethyl acetate, -70 deg C
8: H2O / hydrolysis
9: aluminium chloride / C2H5SH
With
potassium hydroxide; sodium tetrahydroborate; aluminium trichloride; 18-crown-6 ether; dimethylsulfide; mercury(II) diacetate; water; sodium ethanolate; ozone; trifluoroacetic anhydride;
In
1,4-dioxane; ethanol; water; ethanethiol;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 89.1 percent / trifluoroacetic anhydride
2: 1.) mercuric acetate; 2.) sodium borohydride / 1.) water, THF, r.t.
4: 1.) ozon; 2.) dimethyl sulfide / 1.) ethyl acetate, -70 deg C
6: H2O / hydrolysis
7: aluminium chloride / C2H5SH
With
sodium tetrahydroborate; aluminium trichloride; dimethylsulfide; mercury(II) diacetate; water; ozone; trifluoroacetic anhydride;
In
ethanethiol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) mercuric acetate; 2.) sodium borohydride / 1.) water, THF, r.t.
3: 1.) ozon; 2.) dimethyl sulfide / 1.) ethyl acetate, -70 deg C
5: H2O / hydrolysis
6: aluminium chloride / C2H5SH
With
sodium tetrahydroborate; aluminium trichloride; dimethylsulfide; mercury(II) diacetate; water; ozone;
In
ethanethiol;
